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Basic Information
| CAS No.: | 306-44-5 |
|---|---|
| Name: | ISONITROSOACETONE |
| Article Data: | 40 |
| Molecular Structure: | |
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| Formula: | C3H5 N O2 |
| Molecular Weight: | 87.0782 |
| Synonyms: | Pyruvaldehyde,1-oxime (8CI); Pyruvaldehyde, aldoxime (6CI); 2-Oxopropanal 1-oxime;2-Propanone, 1-(hydroxyimino)-; Isonitrosoacetone; MINA; Methylglyoxalaldoxime; Monoisonitrosoacetone; NSC 53172; Pyruvaldoxime; RA 52 |
| Density: | 1.1g/cm3 |
| Melting Point: | 69° |
| Boiling Point: | 193°Cat760mmHg |
| Flash Point: | 70.6°C |
| PSA: | 49.66000 |
| LogP: | 0.03540 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: ethyl acetoacetate With potassium hydroxide In water at 0℃; for 24h; Cooling with ice; Stage #2: With sulfuric acid; sodium nitrite In water at 0 - 20℃; for 2h; pH=4-5; | 79% |
Conditions
| Conditions | Yield |
|---|---|
| With hydroxylamine hydrochloride In tetrahydrofuran; water at 24℃; for 12h; Inert atmosphere; | 79% |
| With hydroxylamine hydrochloride In tetrahydrofuran; water at 20℃; Inert atmosphere; | 65% |
| With pyridine; hydroxylamine hydrochloride; toluene-4-sulfonic acid at 20℃; for 15h; |
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; ethyl nitrite at 45℃; for 1h; | 74% |
| With nitrogen(II) oxide; {pentacyanoferrate(II)}(3-) aq. alkali; | |
| With nitrogen(II) oxide; (OH)pentacyanoferrate(III)(3-) In water catalytic activity of different Fe(III) pentacyano complexes; |
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; diethyl ether |
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride |
Conditions
| Conditions | Yield |
|---|---|
| With nitrosylchloride |
- 1747-09-7, 91775-13-2
1,1'-(Z)-dioxydiazenediyl-bis-propan-2-one
- 306-44-5
propanone 1-oxime
Conditions
| Conditions | Yield |
|---|---|
| In toluene |
- 29456-04-0
propen-2-ol
- 306-44-5
propanone 1-oxime
Conditions
| Conditions | Yield |
|---|---|
| With nitrosylchloride In water at 25℃; Rate constant; | |
| With nitrosyl bromide In water at 25℃; Rate constant; |
