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Basic Information
CAS No.: 111011-78-0
Name: 3-(5,5-diMethyl-2-oxo-1,3,2-dioxaphorinane-2-yl)-4-(3-nitrophenyl)-bu-3-en-2-one
Article Data: 2
Molecular Structure:
Molecular Structure of 111011-78-0 (3-(5,5-diMethyl-2-oxo-1,3,2-dioxaphorinane-2-yl)-4-(3-nitrophenyl)-bu-3-en-2-one)
Formula: C15H18NO6P
Molecular Weight: 339.285
Synonyms: (Z)-3-(5,5-dimethyl-2-oxo-1,3,2λ5-dioxaphosphinan-2-yl)-4-(3-nitrophenyl)but-3-en-2-one
PSA: 108.23000
LogP: 4.31400
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Synthetic route
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3-(dimorpholinomethyl)-1-nitrobenzene

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2-acetonyl-5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinane

111011-78-0

5,5-dimethyl-2-<1-(3-nitrophenyl)-3-oxo-1-buten-2-yl>-2-oxo-1,3,2-dioxaphosphorinane

Conditions
ConditionsYield
With trifluoroacetic acid In toluene 1.) 60 deg C, 30 min, 2.) 0-10 deg C, 3 h;93%
With trifluoroacetic acid In toluene for 2.5h; Ambient temperature;93.2%
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3-nitro-benzaldehyde

111011-80-4

2-acetonyl-5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinane

111011-78-0

5,5-dimethyl-2-<1-(3-nitrophenyl)-3-oxo-1-buten-2-yl>-2-oxo-1,3,2-dioxaphosphorinane

Conditions
ConditionsYield
With piperidine; acetic acid In benzene for 6.5h; Heating;31%
1005-69-2

2-methoxy-5,5-dimethyl-1,3,2-dioxaphosphorinane

111011-78-0

5,5-dimethyl-2-<1-(3-nitrophenyl)-3-oxo-1-buten-2-yl>-2-oxo-1,3,2-dioxaphosphorinane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 65.8 percent / diethyl ether / 7 h / Heating
2: 31 percent / piperidine, acetic acid / benzene / 6.5 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: 65.8 percent / diethyl ether / 7 h / Heating
2: 93.2 percent / trifluoroacetic acid / toluene / 2.5 h / Ambient temperature
View Scheme
126-30-7

2,2-Dimethyl-1,3-propanediol

chromic acid

chromic acid

111011-78-0

5,5-dimethyl-2-<1-(3-nitrophenyl)-3-oxo-1-buten-2-yl>-2-oxo-1,3,2-dioxaphosphorinane

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 33 percent / 100 °C
2: 65.8 percent / diethyl ether / 7 h / Heating
3: 31 percent / piperidine, acetic acid / benzene / 6.5 h / Heating
View Scheme
Multi-step reaction with 3 steps
1: 33 percent / 100 °C
2: 65.8 percent / diethyl ether / 7 h / Heating
3: 93.2 percent / trifluoroacetic acid / toluene / 2.5 h / Ambient temperature
View Scheme

(E)-3-Amino-but-2-enoic acid 1-benzyl-piperidin-3-yl ester

111011-78-0

5,5-dimethyl-2-<1-(3-nitrophenyl)-3-oxo-1-buten-2-yl>-2-oxo-1,3,2-dioxaphosphorinane

5-(5,5-Dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yl)-2,6-dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid 1-benzyl-piperidin-3-yl ester

Conditions
ConditionsYield
In toluene Heating;74%
111011-78-0

5,5-dimethyl-2-<1-(3-nitrophenyl)-3-oxo-1-buten-2-yl>-2-oxo-1,3,2-dioxaphosphorinane

C18(13)CH22N2O2

2-(N-benzyl-N-phenylamino)ethyl 5-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl)-1,4-dihydro-2-<(13)C>methyl-6-methyl-4-(3-nitrophenyl)pyridine-3-carboxylate

Conditions
ConditionsYield
In isopropyl alcohol for 2h; Heating;74%

(E)-3-Amino-but-2-enoic acid 2-{4-[bis-(4-fluoro-phenyl)-methyl]-piperazin-1-yl}-ethyl ester

111011-78-0

5,5-dimethyl-2-<1-(3-nitrophenyl)-3-oxo-1-buten-2-yl>-2-oxo-1,3,2-dioxaphosphorinane

5-(5,5-Dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yl)-2,6-dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid 2-{4-[bis-(4-fluoro-phenyl)-methyl]-piperazin-1-yl}-ethyl ester

Conditions
ConditionsYield
In toluene Heating;62%

(E)-3-Amino-but-2-enoic acid 6-(benzyl-methyl-amino)-hexyl ester

111011-78-0

5,5-dimethyl-2-<1-(3-nitrophenyl)-3-oxo-1-buten-2-yl>-2-oxo-1,3,2-dioxaphosphorinane

5-(5,5-Dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yl)-2,6-dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid 6-(benzyl-methyl-amino)-hexyl ester

Conditions
ConditionsYield
In toluene Heating;61%
54527-73-0

2-ethyl 3-aminocrotonate

111011-78-0

5,5-dimethyl-2-<1-(3-nitrophenyl)-3-oxo-1-buten-2-yl>-2-oxo-1,3,2-dioxaphosphorinane

98908-19-1

2-(N-benzyl-N-methylamino)ethyl 2,6-dimethyl-5-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl)-4-(3-nitrophenyl)-1,4-dihydropyridine-3-carboxylate

Conditions
ConditionsYield
In toluene Heating;60%

(E)-3-Amino-but-2-enoic acid 2-[4-(3-phenyl-propyl)-piperazin-1-yl]-ethyl ester

111011-78-0

5,5-dimethyl-2-<1-(3-nitrophenyl)-3-oxo-1-buten-2-yl>-2-oxo-1,3,2-dioxaphosphorinane

5-(5,5-Dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yl)-2,6-dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid 2-[4-(3-phenyl-propyl)-piperazin-1-yl]-ethyl ester

Conditions
ConditionsYield
In toluene Heating;44%
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    Address:Jian Qiao Community, 789 Shenhua Road, Xihu District, Hangzhou, China, 310000

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  • (Z)-3-(5,5-dimethyl-2-oxo-1,3,2λ5-dioxaphosphinan-2-yl)-4-(3-nitrophenyl)but-3-en-2-one

  • Casno:

    111011-78-0

    (Z)-3-(5,5-dimethyl-2-oxo-1,3,2λ5-dioxaphosphinan-2-yl)-4-(3-nitrophenyl)but-3-en-2-one

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa

    Changzhou Extraordinary Pharmatech co., LTD. Is a full technical team and for the development of hardware and software facilities manufacturing enterprises,The company is located i

  • Changzhou Extraordinary Pharmatech co.,LTD

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86 519 82111935

    Address:Chinese Jiangsu Province Changzhou City Jintan District Jincheng Town Miaotou NO4（Pharmaceutical Park）

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  • 3-(5,5-diMethyl-2-oxo-1,3,2-dioxaphorinane-2-yl)-4-(3-nitrophenyl)-bu-3-en-2-one

  • Casno:

    111011-78-0

    3-(5,5-diMethyl-2-oxo-1,3,2-dioxaphorinane-2-yl)-4-(3-nitrophenyl)-bu-3-en-2-one

    Min.Order: 1 Milligram

    FOB Price:  USD $ 0.0-0.0

    GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

    Xiamen Jenny Chemical Technology Co., Ltd. is a modern high-tech enterprise specializing in the research, production, development, sales and self-support import and export of biolo

  • Xiamen Jenny Chemical Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86 16621006118

    Address:Room 402, No. 216, Nanshan Road, Huli District, Xiamen City

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  • 3-(5,5-diMethyl-2-oxo-1,3,2-dioxaphorinane-2-yl)-4-(3-nitrophenyl)-bu-3-en-2-one

  • Casno:

    111011-78-0

    3-(5,5-diMethyl-2-oxo-1,3,2-dioxaphorinane-2-yl)-4-(3-nitrophenyl)-bu-3-en-2-one

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Zhejiang Jiuzhou Chem Co.,Ltd is a foreign trading company, specializing in developing and producing Organic intermediate . It has its own factory, which procures itself a competitive edge in market. For many years, our company has won many clients&

    Zhejiang Jiuzhou Chem Co.,Ltd is a market-oriented and innovation-driven biopharmaceutical company. The company is focusing on the R&D, manufacturing and sales of pharmaceutical pr

  • ZHEJIANG JIUZHOU CHEM CO.,LTD

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86 19334956669-956-669

    Address:Waisha Road,Jiaojiang

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  • 3-(5,5-diMethyl-2-oxo-1,3,2-dioxaphorinane-2-yl)-4-(3-nitrophenyl)-bu-3-en-2-one

  • Casno:

    111011-78-0

    3-(5,5-diMethyl-2-oxo-1,3,2-dioxaphorinane-2-yl)-4-(3-nitrophenyl)-bu-3-en-2-one

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    High quality, competitive price, fast delivery and first-class service we possesses have won the trust and praise of customers. Standard: BP/USP/EP The purity is equal or greater than 99%. As a supplier, we can provide high-quality produc

    Henan Kanbei Chemical Co., Ltd. is a modern high-tech chemical enterprise integrating R&D, production and sales. The company has strong technical strength, advanced equipment, stri

  • Henan Kanbei Chemical Co.,LTD

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-152-37804566

    Address:Evergrande Future City, intersection of Zhengkai Avenue and Sixteenth Street, Kaifeng Area, Henan Pilot Free Trade Zone

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  • 3-(5,5-Dimethyl-2-Oxo-1,3,2-Dioxaphorinane-2-Yl)-4-(3-Nitrophenyl)-Bu-3-En-2-One

  • Casno:

    111011-78-0

    3-(5,5-Dimethyl-2-Oxo-1,3,2-Dioxaphorinane-2-Yl)-4-(3-Nitrophenyl)-Bu-3-En-2-One

    Min.Order: 100 Gram

    FOB Price:  USD $ 0.0-0.0

    Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

    Jinhua huayi chemical co., ltd. has own manufacturers which focus on production of organic specialty products,Pharmaceuticals and its intermediates,fine chemcals of high purity.The

  • JINHUA HUAYI CHEMICAL CO., LTD.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-579-82660891

    Address:47-204 No.288, Shida St., Wuchem Dist., Jinhua,Zhejiang, 321004 China

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  • 3-Buten-2-one, 3-(5,5-dimethyl-2-oxido-1,3,2-dioxaphosphorinan-2-yl)-4-(3-nitrophenyl)- (9CI)

  • Casno:

    111011-78-0

    3-Buten-2-one, 3-(5,5-dimethyl-2-oxido-1,3,2-dioxaphosphorinan-2-yl)-4-(3-nitrophenyl)- (9CI)

    Min.Order: 1 Metric Ton

    FOB Price:  USD $ 1.0-2.0

    Strict quality control system and PHD We has passed through the ISO9001:2016 Quality System Certificate, we have strict quality control system. we have about 300 employees, including 90 full-time PHD 15 PHD and masters above, 153 undergraduates, wi

    Hubei Ipure biotech Co., Ltd. is Established in 2011,which is located in Wuhan, Hubei Province where is the largest city in central China. The company is a diversified product pr

  • HuBei Ipure Biotech CO.,ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:18062427325

    Address:NO 18. 81F street Future city ,Hongshan district ,WuHan city ,Hubei province ,China

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