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118684-17-6

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118684-17-6 Usage

Check Digit Verification of cas no

The CAS Registry Mumber 118684-17-6 includes 9 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 6 digits, 1,1,8,6,8 and 4 respectively; the second part has 2 digits, 1 and 7 respectively.
Calculate Digit Verification of CAS Registry Number 118684-17:
(8*1)+(7*1)+(6*8)+(5*6)+(4*8)+(3*4)+(2*1)+(1*7)=146
146 % 10 = 6
So 118684-17-6 is a valid CAS Registry Number.

118684-17-6Relevant articles and documents

Additive-freeN-methylation of amines with methanol over supported iridium catalyst

Liu, Xiang,Loh, Teck-Peng,Qiang, Wenwen,Wang, Jing,Ye, Sen,Zhu, Longfei

, p. 3364 - 3375 (2021/06/06)

An efficient and versatile zinc oxide-supported iridium (Ir/ZnO) catalyst was developed to catalyze the additive-freeN-methylation of amines with methanol. Mechanistic studies suggested that the high catalytic reactivity is rooted in the small sizes (1.4 nm) of Ir nanoparticles and the high ratio (93%) of oxidized iridium species (IrOx, Ir3+and Ir4+) on the catalyst. Moreover, the delicate cooperation between the IrOxand ZnO support also promoted its high reactivity. The selectivity of this catalyticN-methylation was controllable between dimethylation and monomethylation by carefully tuning the catalyst loading and reaction solvent. Specifically, neat methanol with high catalyst loading (2 mol% Ir) favored the formation ofN,N-dimethylated amine, while the mesitylene/methanol mixture with low catalyst loading (0.5 mol% Ir) was prone to producing mono-N-methylated amines. An environmentally benign continuous flow system with a recycled mode was also developed for the efficient production ofN-methylated amines. With optimal flow rates and amine concentrations, a variety ofN-methylamines were produced with good to excellent yields in this Ir/ZnO-based flow system, providing a starting point for the clean and efficient production ofN-methylamines with this cost-effective chemical process.

Two consecutive palladium(II)-promoted C-H alkenylation reactions for the synthesis of 3-alkenylquinolones

Ortiz-de-Elguea, Vernica,Sotomayor, Nuria,Lete, Esther

, p. 463 - 473 (2015/03/05)

Highly substituted quinolones are obtained through an efficient and atom economical procedure that involves two consecutive palladium(II)-catalyzed C-H alkenylation reactions. A selective 6-endo intramolecular C-H alkenylation leads to 4-substituted quinolones that have been further functionalized at C-3 through a second intermolecular C-H alkenylation reaction.

Synthesis and biological evaluation of 2-phenylquinolones targeted at Tat/TAR recognition

Manfroni, Giuseppe,Gatto, Barbara,Tabarrini, Oriana,Sabatini, Stefano,Cecchetti, Violetta,Giaretta, Giulia,Parolin, Cristina,Del Vecchio, Claudia,Calistri, Arianna,Palumbo, Manlio,Fravolini, Arnaldo

supporting information; experimental part, p. 714 - 717 (2009/08/15)

Tat (transactivator of transcription) is a small HIV protein rich in arginines that interacts with a viral RNA structure called TAR (trans-activation responsive region). Tat-TAR interaction is essential for viral gene expression, replication and pathogene

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