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Basic Information
| CAS No.: | 89-55-4 |
|---|---|
| Name: | 5-Bromosalicylic acid |
| Article Data: | 72 |
| Molecular Structure: | |
|
|
|
| Formula: | C7H5BrO3 |
| Molecular Weight: | 217.019 |
| Synonyms: | Salicylicacid, 5-bromo- (6CI,8CI);2-Hydroxy-5-bromobenzoic acid;5-Bromo-2-hydroxybenzoic acid;NSC 3981;NSC 52393; |
| EINECS: | 201-917-0 |
| Density: | 1.861 g/cm3 |
| Melting Point: | 162-166 °C |
| Boiling Point: | 338.1 °C at 760 mmHg |
| Flash Point: | 158.3 °C |
| Solubility: | Soluble in water |
| Appearance: | white to slightly beige powder |
| Hazard Symbols: |
 Xi
|
| Risk Codes: | 36/37/38 |
| Safety: | 37/39-26-36 |
| PSA: | 57.53000 |
| LogP: | 1.85290 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With tetrapropylammonium nonabromide In dichloromethane at 23℃; for 0.5h; Inert atmosphere; | 95% |
| With sodium vanadate; aluminum tri-bromide; tetrabutylammomium bromide; oxygen In 1,4-dioxane; water at 80℃; for 8h; Reagent/catalyst; Solvent; Temperature; | 93.1% |
| With 1-butyl-3-methylpyridinium tribromide at 20℃; for 1h; | 89% |
Conditions
| Conditions | Yield |
|---|---|
| With sodium chlorite; sodium methylate In dimethyl sulfoxide | 84% |
- 21740-00-1
5-bromo-2-iodo-benzoic acid
- 89-55-4
5-bromosalicyclic acid
Conditions
| Conditions | Yield |
|---|---|
| With copper(I) oxide; 1-D-O-Methyl-chiro-inositol; sodium hydroxide In water at 100℃; for 6h; | 77% |
- 82486-43-9
2-hydroxy-5-bromobenzaldehyde oxime
A
- 89-55-4
5-bromosalicyclic acid
B
- 1761-61-1
5-bromosalicyclaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With calcium hypochlorite; montmorillonite K-10 In chloroform at 20℃; for 4h; | A 2.5% B 69% |
A
- 5827-78-1
N-methyl-N-phenylpropanamide
B
- 89-55-4
5-bromosalicyclic acid
C
- 17764-93-1
5-bromo-2-hydroxypropiophenone
Conditions
| Conditions | Yield |
|---|---|
| With water; sodium hydride In tetrahydrofuran for 24h; Reflux; | A 60% B 43% C n/a |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide |
- 109-72-8, 29786-93-4
n-butyllithium
- 60-29-7
diethyl ether
- 615-58-7
2,4-dibromophenol
- 89-55-4
5-bromosalicyclic acid
Conditions
| Conditions | Yield |
|---|---|
| anschliessend Behandeln mit festem Kohlendioxid; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With n-butyllithium; diethyl ether anschliessendes Behandeln mit CO2; |
- 10268-63-0
phenyl 5-bromo-2-hydroxybenzoate
- 89-55-4
5-bromosalicyclic acid
Conditions
| Conditions | Yield |
|---|---|
| bei der Verseifung; |
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide |
Raw Materials
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5-Bromosalicylic acid
Chemistry
5-Bromosalicylic acid(89-55-4) is the chemical compound with the formula C7H5BrO3.Its molar weight is 217.02g/mol.
5-Bromosalicylic acid(89-55-4) is also named 2-Hydroxy-5-bromobenzoic acid;3-bromo-6-hydroxy-benzoicaci;5-bromo-2-hydroxy-benzoicaci;5-bromo-salicylicaci;Benzoic acid, 3-bromo-6-hydroxy-;Benzoic acid, 5-bromo-2-hydroxy-;Benzoicacid,5-bromo-2-hydroxy-;Salicylic acid, 5-bromo-.
Melting Point: 162-166 oC
Boiling Point: 338.1 oC at 760 mmHg
Flash Point: 158.3 oC
Water Solubility: Soluble
Index of Refraction: 1.654
Molar Refractivity: 42.75 cm3
Molar Volume: 116.5 cm3
Surface Tension: 68.1 dyne/cm
Density: 1.861 g/cm3
Enthalpy of Vaporization: 61.36 kJ/mol
Vapour Pressure: 3.93E-05 mmHg at 25 oC
The chemical structure of 5-Bromosalicylic acid(89-55-4) is
.
5-Bromosalicylic acid(89-55-4) is also named 2-Hydroxy-5-bromobenzoic acid;3-bromo-6-hydroxy-benzoicaci;5-bromo-2-hydroxy-benzoicaci;5-bromo-salicylicaci;Benzoic acid, 3-bromo-6-hydroxy-;Benzoic acid, 5-bromo-2-hydroxy-;Benzoicacid,5-bromo-2-hydroxy-;Salicylic acid, 5-bromo-.
Melting Point: 162-166 oC
Boiling Point: 338.1 oC at 760 mmHg
Flash Point: 158.3 oC
Water Solubility: Soluble
Index of Refraction: 1.654
Molar Refractivity: 42.75 cm3
Molar Volume: 116.5 cm3
Surface Tension: 68.1 dyne/cm
Density: 1.861 g/cm3
Enthalpy of Vaporization: 61.36 kJ/mol
Vapour Pressure: 3.93E-05 mmHg at 25 oC
The chemical structure of 5-Bromosalicylic acid(89-55-4) is
.Uses
5-Bromosalicylic acid(89-55-4) is used as organic synthesis.
Toxicity Data With Reference
| 1. | ivn-mus LD50:100 mg/kg | CSLNX* U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. (Aberdeen Proving Ground, MD 21010) NX#04478 . |
Consensus Reports
Reported in EPA TSCA Inventory.
Safety Profile
Poison by intravenous route. When heated to decomposition it emits toxic fumes of Br−.
Hazard Codes:
Xi
Risk Statements: 36/37/38
36/37/38: Irritating to eyes, respiratory system and skin
Safety Statements: 37/39-26-36
37/39: Wear suitable gloves and eye/face protection
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
RTECS: VO1850000.
Hazard Codes:
Xi Risk Statements: 36/37/38
36/37/38: Irritating to eyes, respiratory system and skin
Safety Statements: 37/39-26-36
37/39: Wear suitable gloves and eye/face protection
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
RTECS: VO1850000.
Specification
5-Bromosalicylic acid(89-55-4)The extinguishing agents of 5-Bromosalicylic acid(89-55-4) is dry powder, carbon dioxide, water mist.