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| CAS No.: | 86087-23-2 |
|---|---|
| Name: | (S)-(+)-3-Hydroxytetrahydrofuran |
| Article Data: | 28 |
| Molecular Structure: | |
|
|
|
| Formula: | C4H8O2 |
| Molecular Weight: | 88.1063 |
| Synonyms: | 3-Furanol,tetrahydro-, (S)-;(+)-3-Hydroxytetrahydrofuran;(S)-(+)-Tetrahydrofuran-3-ol;(S)-3-Hydroxytetrahydrofuran;(S)-Tetrahydro-3-furanol;3S-Hydroxytetrahydrofuran; |
| EINECS: | 1308068-626-2 |
| Density: | 1.148 g/cm3 |
| Boiling Point: | 181 °C at 760 mmHg |
| Flash Point: | 81.1 °C |
| Solubility: | soluble in water |
| Appearance: | clear liquid |
| Hazard Symbols: |
 Xi
|
| Risk Codes: | 36/37/38 |
| Safety: | 26-37/39 |
| PSA: | 29.46000 |
| LogP: | -0.23240 |
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(3S)-4-chloro-1,3-butanediol
- 86087-23-2
(S)-3-hydroxytetyrahydrofurane
| Conditions | Yield |
|---|---|
| With hydrogenchloride; sodium hydroxide In methanol; water | 99.8% |
| With potassium hydroxide In methanol at 40℃; for 4h; Reagent/catalyst; | 97% |
| In anhydrous ethylene glycol dimethyl ether at 110℃; for 5h; Product distribution / selectivity; | 90% |
- 145873-44-5
4-chloro-3-hydroxy-1-butanol
- 86087-23-2
(S)-3-hydroxytetyrahydrofurane
| Conditions | Yield |
|---|---|
| With hydrogenchloride In water at 50℃; for 4h; Solvent; Reagent/catalyst; | 94.6% |
A
- 83318-92-7
ethyl p-methoxybenzyl sulfide
B
- 86087-23-2
(S)-3-hydroxytetyrahydrofurane
| Conditions | Yield |
|---|---|
| With aluminium trichloride; ethanethiol In dichloromethane for 5h; Ambient temperature; | A n/a B 93% |
- 42890-76-6
(S)-1,2,4-butanetriol
- 86087-23-2
(S)-3-hydroxytetyrahydrofurane
| Conditions | Yield |
|---|---|
| With toluene-4-sulfonic acid (3a preparation above 7a); | 87% |
| toluene-4-sulfonic acid In PEG-400 at 120 - 160℃; under 10 Torr; for 12h; Product distribution / selectivity; | 83% |
| strong acid ion exchange resin (Amberlyst 15, H+ form) In 1,4-dioxane at 90 - 120℃; under 760.051 - 5931.67 Torr; Product distribution / selectivity; | 70% |
| With toluene-4-sulfonic acid | |
| With toluene-4-sulfonic acid In water at 90℃; | 10 g |
- 86087-23-2
(S)-3-hydroxytetyrahydrofurane
| Conditions | Yield |
|---|---|
| With sodium hydroxide In methanol; water at 20℃; for 3h; | 83% |
- 86087-23-2
(S)-3-hydroxytetyrahydrofurane
| Conditions | Yield |
|---|---|
| With palladium on activated charcoal; hydrogen at 40℃; | 81.5% |
- 86087-24-3
(R)-3-Hydroxytetrahydrofuran
- 86087-23-2
(S)-3-hydroxytetyrahydrofurane
| Conditions | Yield |
|---|---|
| Stage #1: (R)-3-Hydroxytetrahydrofuran With azodicarboxylic acid bis(2-methoxyethyl) ester; 4-diphenylphosphanobenzoic acid In tetrahydrofuran at 20℃; for 0.166667h; Stage #2: With water; sodium hydroxide In tetrahydrofuran at 20℃; stereospecific reaction; | 64% |
- 115914-74-4
2-(oxiran-2-yl)ethyl 4-methylbenzenesulfonate
A
- 86087-23-2
(S)-3-hydroxytetyrahydrofurane
| Conditions | Yield |
|---|---|
| With (S,S)-(salen)cobalt(III)(OAc); water In tetrahydrofuran at 0 - 25℃; for 14h; optical yield given as %ee; enantioselective reaction; | A 48% B 47% |
- 1191-99-7
2,3-dihydro-2H-furan
- 86087-23-2
(S)-3-hydroxytetyrahydrofurane
| Conditions | Yield |
|---|---|
| Yield given. Multistep reaction; |
- 1708-29-8
2,5-dihydrofuran
- 86087-23-2
(S)-3-hydroxytetyrahydrofurane
| Conditions | Yield |
|---|---|
| Multistep reaction; | |
| Yield given. Multistep reaction; |
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Chemistry
Product Name: (S)-(+)-3-Hydroxytetrahydrofuran (CAS NO.86087-23-2)
Molecular Formula: C4H8O2
Molecular Weight: 88.11g/mol
Mol File: 86087-23-2.mol
Appearance: Colourless Liquid
Boiling point: 181 °C at 760 mmHg
Flash Point: 81.1 °C
Density: 1.148 g/cm3
Refractive index: n20/D 1.45(lit.)
Water Solubility: soluble
Stability: Stable. Combustible. Incompatible with strong oxidizing agents.
Index of Refraction: 1.475
Molar Refractivity: 21.64 cm3
Molar Volume: 76.7 cm3
Surface Tension: 38.7 dyne/cm
Enthalpy of Vaporization: 48.57 kJ/mol
Vapour Pressure: 0.255 mmHg at 25°C
Product Categories: Alcohols, Hydroxy Esters and Derivatives; Chiral Compounds; Starting Raw Materials & Intermediates; Small molecule; Tetrahydrofuran Series; Chiral Reagents; Furans; Chiral Building Blocks; Simple Alcohols (Chiral); Synthetic Organic Chemistry
Safety Profile
Safety Information of (S)-(+)-3-Hydroxytetrahydrofuran (CAS NO.86087-23-2):
Hazard Codes: Xi
Risk Statements: 36/37/38
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-37/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S37/39:Wear suitable gloves and eye/face protection.
WGK Germany: 3
Specification
(S)-(+)-3-Hydroxytetrahydrofuran , its CAS NO. is 86087-23-2, the synonyms are (3S)-tetrahydrofuran-3-ol ; (S)-(+)-Tetrahydro-3-furanol .
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