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Basic Information
| CAS No.: | 67330-62-5 |
|---|---|
| Name: | 3-CHLORO-2,6-DIETHYLANILINE |
| Molecular Structure: | |
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|
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| Formula: | C10H14 Cl N |
| Molecular Weight: | 183.681 |
| Synonyms: | Aniline,3-chloro-2,6-diethyl- (6CI); 3-Chloro-2,6-diethylaniline;3-Chloro-2,6-diethylbenzenamine |
| Density: | 1.095g/mLat 25°C(lit.) |
| Boiling Point: | 137-139°C10mm Hg(lit.) |
| Flash Point: | >230°F |
| Hazard Symbols: | Xn |
| Risk Codes: | 20/21/22-36/37/38 |
| PSA: | 26.02000 |
| LogP: | 3.62820 |
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Synthetic route
- 104851-50-5
acetic acid-(2,6-diethyl-3-chloro-anilide)
- 67330-62-5
2,6-diethyl-3-chloro-aniline
Conditions
| Conditions | Yield |
|---|---|
| With sulfuric acid |
Conditions
| Conditions | Yield |
|---|---|
| With aluminium | |
| With aluminium trichloride; aluminium | |
| With aluminium trichloride; aluminium at 250℃; under 147837 Torr; |
- 16665-89-7
N-(2,6-diethylphenyl)acetamide
- 67330-62-5
2,6-diethyl-3-chloro-aniline
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: acetic acid; chlorine 2: aqueous H2SO4 View Scheme | |
| Multi-step reaction with 3 steps 1: aqueous KClO 2: acetic acid 3: aqueous H2SO4 View Scheme |
- 104851-74-3
acetic acid-(2,6-diethyl-N-chloro-anilide)
- 67330-62-5
2,6-diethyl-3-chloro-aniline
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: acetic acid 2: aqueous H2SO4 View Scheme |
- 579-66-8
2,6-diethylaniline
- 67330-62-5
2,6-diethyl-3-chloro-aniline
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 2,6-diethylaniline With sulfuric acid; chlorine at 30℃; for 3h; Autoclave; Stage #2: With sodium hydroxide In water Product distribution / selectivity; | 94.4 %Chromat. |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 2,6-diethylaniline With sulfuric acid; chlorine at 35℃; for 4.5h; autoclave; Stage #2: With sodium hydroxide In water | A 8.3 %Chromat. B 71.2 %Chromat. |
| Stage #1: 2,6-diethylaniline With chlorosulfonic acid; chlorine at 30℃; for 3h; autoclave; Stage #2: With sodium hydroxide In water | A 18.6 %Chromat. B 10.5 %Chromat. |
- 54616-46-5
2-Iodo-N,N-dimethylbenzamide
- 67330-62-5
2,6-diethyl-3-chloro-aniline
- 269061-78-1
2-(3-chloro-2,6-diethyl-phenylamino)-N,N-dimethyl-benzamide
Conditions
| Conditions | Yield |
|---|---|
| With copper(l) iodide; copper; potassium carbonate In xylene Condensation; Heating; | 58% |
- 67330-62-5
2,6-diethyl-3-chloro-aniline
- 916585-89-2
3-chloro-2,6-diethyl-5-nitro-phenylamine
Conditions
| Conditions | Yield |
|---|---|
| With sulfuric acid; nitric acid at 0℃; for 2.5h; | 50% |
- 67330-62-5
2,6-diethyl-3-chloro-aniline
- 872271-34-6
7-hydroxy-naphthalene-1,3-disulfonyl chloride
Conditions
| Conditions | Yield |
|---|---|
| In acetonitrile for 4h; Heating / reflux; | 4% |
- 463-71-8
thiophosgene
- 67330-62-5
2,6-diethyl-3-chloro-aniline
- 67330-49-8
3-Chlor-2,6-diaethyl-phenylisothiocyanat
Conditions
| Conditions | Yield |
|---|---|
| With calcium carbonate In dichloromethane; water | |
| With water; calcium carbonate | |
| With water; calcium carbonate In dichloromethane Heating; | |
| With water; calcium carbonate In dichloromethane |
