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Basic Information
CAS No.: 6485-57-0
Name: 2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone
Article Data: 26
Molecular Structure:
Molecular Structure of 6485-57-0 (2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone)
Formula: C15H24 O3
Molecular Weight: 252.354
Synonyms: 2,5-Cyclohexadien-1-one,2,6-di-tert-butyl-4-hydroperoxy-4-methyl- (8CI); Hydroperoxide,3,5-di-tert-butyl-1-methyl-4-oxo-2,5-cyclohexadien-1-yl (6CI,7CI);2,6-Di-tert-butyl-4-methyl-4-hydroperoxy-2,5-cyclohexadiene-1-one;4-Hydroperoxy-4-methyl-2,6-di-tert-butyl-2,5-cyclohexadienone;4-Methyl-4-hydroperoxy-2,6-di-tert-butyl-2,5-cyclohexadienone
Density: 1.02g/cm3
Boiling Point: 360.6°Cat760mmHg
Flash Point: 125°C
PSA: 46.53000
LogP: 3.76240
Related products
Synthetic route
128-37-0

2,6-di-tert-butyl-4-methyl-phenol

6485-57-0

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions
ConditionsYield
With methylene blue In methanol; water under 7500.75 Torr; for 0.266667h; Irradiation; Flow reactor;99%
With 2,8-dibromo-5,5-difluoro-1,3,7,9-tetramethyl-10-phenyl-5H-dipyrrolo[1,2-c:2′,1′-f ][1,3,2]diazaborinin-4-ium-5-uide; oxygen In 1,4-dioxane for 6h; Irradiation;95%
With potassium hydroxide; oxygen
128-37-0

2,6-di-tert-butyl-4-methyl-phenol

A

52922-83-5

1,3-di-tert-butyl-5-hydroxy-5-methyl-7-oxabicyclo[4.1.0]hept-3-en-2-one

B

6485-57-0

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions
ConditionsYield
With (3-)*3Et4N(1+); oxygen In N,N-dimethyl-formamide at 0℃; for 2h;A 9%
B 91%
67-56-1

methanol

128-37-0

2,6-di-tert-butyl-4-methyl-phenol

93-55-0

1-phenyl-propan-1-one

A

16735-22-1

3-hydroxy-2-methylpropiophenone

B

10396-80-2

2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone

C

6485-57-0

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions
ConditionsYield
With 4,5,6,7-tetrachloro-2',4',5',7'-tetraiodofluorescein disodium salt; potassium carbonate In water at 20℃; for 36h; Irradiation;A 12%
B 60%
C 17%
...Expand
128-37-0

2,6-di-tert-butyl-4-methyl-phenol

A

10396-80-2

2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone

B

6485-57-0

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions
ConditionsYield
With 1-([1,1'-biphenyl]-2-yl)propan-1-one; oxygen; rose bengal; potassium carbonate at 20℃; for 34h; Irradiation;A 57%
B 18%
With 9,10-Dicyanoanthracene; oxygen In acetonitrile for 55h; Rate constant; Product distribution; Mechanism; Irradiation;
With 9,10-Dicyanoanthracene; oxygen In acetonitrile for 55h; Irradiation; Yield given. Yields of byproduct given;
128-37-0

2,6-di-tert-butyl-4-methyl-phenol

137-07-5

2-amino-benzenethiol

611-73-4

Benzoylformic acid

A

883-93-2

2-Phenylbenzothiazole

B

6485-57-0

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

C

C29H33NO3S

Conditions
ConditionsYield
With dihydrogen peroxide In 1,4-dioxane; water at 20℃; for 8h; Irradiation;A 38%
B n/a
C n/a
...Expand
128-37-0

2,6-di-tert-butyl-4-methyl-phenol

A

719-22-2

2,6-Di-tert-butyl-1,4-benzoquinone

B

10396-80-2

2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone

C

6485-57-0

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions
ConditionsYield
With dihydrogen peroxide; phosphomolybdic acid In acetic acid at 30℃; for 5h; Product distribution; other heteropolyacids as catalyst;A 4.1%
B 1.7%
C 34.1%
...Expand
128-37-0

2,6-di-tert-butyl-4-methyl-phenol

A

719-22-2

2,6-Di-tert-butyl-1,4-benzoquinone

B

2455-14-3

3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone

C

10396-80-2

2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone

D

6485-57-0

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

E

14387-13-4

2,6-di-tert-butyl-4-(3,5-di-tert-butyl-4-hydroxyphenyl)-4-methyl-2,5-cyclohexadiene-1-one

F

1620-98-0

3,5-di-t-butyl-4-hydroxybenzaldehyde

Conditions
ConditionsYield
With ammonia; oxygen In propan-1-ol; water at 88℃; for 1h; Product distribution; oth. time, oth. temperature;A 3.5%
B 2.1%
C 14%
D 17%
E 8.8%
F 1.5%
...Expand
6858-01-1, 24473-56-1

2,6-di-tert-butyl-4-methylphenoxy radical

A

128-37-0

2,6-di-tert-butyl-4-methyl-phenol

B

6485-57-0

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions
ConditionsYield
With C5CoN5O2(3-)*3C36H30NP2(1+) In dichloromethane at -70℃; for 0.0833333h; starting material added in dimer form; Title compound not separated from byproducts;A 30 % Chromat.
B 70 % Chromat.
62926-71-0

Ethaneperoxoic acid 3,5-di-tert-butyl-1-methyl-4-oxo-cyclohexa-2,5-dienyl ester

6485-57-0

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions
ConditionsYield
With trifluoroacetic acid In methanol
99-65-0

meta-dinitrobenzene

128-37-0

2,6-di-tert-butyl-4-methyl-phenol

oxygen

oxygen

aq.-ethanolic KOH

aq.-ethanolic KOH

6485-57-0

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions
ConditionsYield
at -10 - 40℃; Rate constant;
...Expand
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