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62396-98-9

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Basic Information
CAS No.: 62396-98-9
Name: α-Oxo-1,3-benzodioxole-5-acetic Acid
Article Data: 20
Molecular Structure:
Molecular Structure of 62396-98-9 (α-Oxo-1,3-benzodioxole-5-acetic Acid)
Formula: C9H6O5
Molecular Weight: 194.144
Synonyms: Benzo[1,3]dioxol-5-yl-glyoxylsaeure;Alpha-Oxo-1,3-benzodioxole-5-acetic Acid;benzo[1,3]dioxol-5-yl-glyoxylic acid;α-Oxo-1,3-benzodioxole-5-acetic Acid;
Density: 1.531±0.06 g/cm3(Predicted)
Boiling Point: 366.2±42.0 °C(Predicted)
PSA: 72.83000
LogP: 0.68260
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Synthetic route
86358-30-7

benzo[1,3]dioxol-5-ylglyoxylic acid ethyl ester

62396-98-9

benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions
ConditionsYield
Stage #1: benzo[1,3]dioxol-5-ylglyoxylic acid ethyl ester With methanol; sodium hydroxide at 0℃; for 2h;
Stage #2: In water pH=~ 3 - 4;		70%
With water; lithium hydroxide In tetrahydrofuran at 20℃; for 3h; Inert atmosphere;32%
With water; sodium hydroxide In tetrahydrofuran for 6h; Reflux;
With sodium hydroxide In water at 0 - 20℃; for 6h;
3162-29-6

1-(benzo[d][1,3]dioxol-6-yl)ethanone

62396-98-9

benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions
ConditionsYield
With pyridine; selenium(IV) oxide at 90 - 110℃; for 4h; Inert atmosphere;39%
With potassium permanganate
With pyridine; selenium(IV) oxide

2-(benzo[d][1,3]dioxol-5-yl)-N-methyl-2-oxoacetamide

62396-98-9

benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions
ConditionsYield
With sodium hydroxide
120-58-1

isosafrole

A

94-53-1

Piperonylic acid

B

62396-98-9

benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions
ConditionsYield
With potassium permanganate; water
3162-29-6

1-(benzo[d][1,3]dioxol-6-yl)ethanone

alkaline potassium permanganate

alkaline potassium permanganate

62396-98-9

benzo[1,3]dioxol-5-yl-oxo-acetic acid

90843-60-0

2-(3,4-dioxymethylenephenyl)propionaldehyde

alkaline potassium permanganate

alkaline potassium permanganate

62396-98-9

benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions
ConditionsYield
in der Kaelte;
3162-29-6

1-(benzo[d][1,3]dioxol-6-yl)ethanone

alkaline potassium permanganate

alkaline potassium permanganate

A

94-53-1

Piperonylic acid

B

62396-98-9

benzo[1,3]dioxol-5-yl-oxo-acetic acid

...Expand
120-58-1

isosafrole

aqueous potassium permanganate

aqueous potassium permanganate

A

94-53-1

Piperonylic acid

B

62396-98-9

benzo[1,3]dioxol-5-yl-oxo-acetic acid

...Expand
120-58-1

isosafrole

aqueous potassium permanganate

aqueous potassium permanganate

A

94-53-1

Piperonylic acid

B

62396-98-9

benzo[1,3]dioxol-5-yl-oxo-acetic acid

C

3.4-methylenedioxy-mandelic acid

3.4-methylenedioxy-mandelic acid

...Expand
25054-53-9

3,4-(methylenedioxy)benzoyl chloride

62396-98-9

benzo[1,3]dioxol-5-yl-oxo-acetic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 90 °C / Durchleiten von Wasserdampf durch das in Chloroform und Benzol geloeste Reaktionsprodukt
2: NaOH-solution
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