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Basic Information
CAS No.: 59467-77-5
Name: Climazolam
Article Data: 5
Molecular Structure:
Molecular Structure of 59467-77-5 (Climazolam)
Formula: C18H13 Cl2 N3
Molecular Weight: 342.227
Synonyms: Climazolam;Ro 21-3982
Density: 1.38g/cm3
Boiling Point: 522.7°C at 760 mmHg
Flash Point: 269.9°C
PSA: 30.18000
LogP: 4.27410
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Synthetic route
59467-76-4

8-chloro-6-(2-chlorophenyl)-3a,4-dihydro-1-methyl-4H-imidazo[1,5-a][1,4]benzodiazepine

59467-77-5

8-chloro-6-(2-chloro-phenyl)-1-methyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

Conditions
ConditionsYield
With enzyme-containing bacterial cell from Arthrobacter sp. at 25℃; for 35h; pH=6.5; Concentration; Enzymatic reaction;89%
With manganese dioxide In toluene

2-aminomethyl-7-chloro-5-(2-chlorophenyl)-2,3-dihydro-1H-1,4-benzodiazepine

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8-chloro-6-(2-chloro-phenyl)-1-methyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 3 h / Sonication
2: enzyme-containing bacterial cell from Arthrobacter sp. / 35 h / 25 °C / pH 6.5 / Enzymatic reaction
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