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Basic Information
| CAS No.: | 588-46-5 |
|---|---|
| Name: | N-BENZYLACETAMIDE |
| Article Data: | 489 |
| Molecular Structure: | |
|
|
|
| Formula: | C9H11 N O |
| Molecular Weight: | 149.192 |
| Synonyms: | Acetamide,N-benzyl- (6CI,7CI,8CI); N-(Phenylmethyl)acetamide; N-Acetylbenzylamine;N-Benzylacetamide; NSC 8065 |
| Density: | 1.031g/cm3 |
| Melting Point: | 61°C |
| Boiling Point: | 157 °C / 2mmHg |
| Flash Point: | 194.5°C |
| PSA: | 29.10000 |
| LogP: | 1.71360 |
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Synthetic route
- 104293-02-9
1-ethoxy-2-(trimethylsilyl)vinyl acetate
- 100-46-9
benzylamine
- 588-46-5
N-(phenylmethyl)acetamide
Conditions
| Conditions | Yield |
|---|---|
| In dichloromethane at 20℃; for 1.5h; | 100% |
Conditions
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 40℃; for 1h; through a column packed with the powdere polymer; | 100% |
Conditions
| Conditions | Yield |
|---|---|
| With Trimethylacetic acid at 90℃; for 24h; Inert atmosphere; chemoselective reaction; | 100% |
| With iron(III) chloride In neat (no solvent) at 80℃; Catalytic behavior; Temperature; Reagent/catalyst; Sealed tube; | 99% |
| for 0.2h; Heating; | 97% |
Conditions
| Conditions | Yield |
|---|---|
| With potassium carbonate In methanol; dichloromethane at 25℃; for 1h; | 100% |
- 3240-34-4
[bis(acetoxy)iodo]benzene
- 603-35-0
triphenylphosphine
- 100-46-9
benzylamine
A
- 588-46-5
N-(phenylmethyl)acetamide
B
- 791-28-6
Triphenylphosphine oxide
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: [bis(acetoxy)iodo]benzene; triphenylphosphine In chloroform for 1h; Heating; Stage #2: benzylamine In chloroform for 0.166667h; | A 94% B 100% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| In neat (no solvent) at 20℃; for 3h; Green chemistry; | 100% |
| at 60℃; for 3h; |
Conditions
| Conditions | Yield |
|---|---|
| In ethanol for 3h; Ambient temperature; | 99% |
Conditions
| Conditions | Yield |
|---|---|
| With indium; sodium dodecyl-sulfate at 20℃; for 20h; | 99% |
- 2735-73-1
1,3-diacetyl-1,3-dihydro-benzoimidazol-2-one
- 100-46-9
benzylamine
A
- 588-46-5
N-(phenylmethyl)acetamide
B
- 14394-91-3
1-acetyl-1,3-dihydro-2H-benzoimidazol-2-one
Conditions
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 20℃; for 0.416667h; | A 99% B n/a |
...Expand
- 1363906-80-2
1-acetyl-2,3,4,6,7,8-hexahydropyrrolo[1,2-a]pyrimidinium tetraphenylborate
- 100-46-9
benzylamine
- 588-46-5
N-(phenylmethyl)acetamide
Conditions
| Conditions | Yield |
|---|---|
| In acetonitrile at 80℃; for 1h; Inert atmosphere; | 99% |
