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Basic Information
| CAS No.: | 528-71-2 |
|---|---|
| Name: | 1-HYDROXYPHENAZINE |
| Article Data: | 36 |
| Molecular Structure: | |
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|
|
| Formula: | C12H8 N2 O |
| Molecular Weight: | 196.208 |
| Synonyms: | Hemipyocyanine(6CI); 1-Hydroxy-9,10-diazaanthracene; 1-Hydroxyphenazine; Hemipyocyanin; NSC88882; Pyoxanthose; a-Hydroxyphenazine |
| Density: | 1.1788 (rough estimate) |
| Melting Point: | 158°C |
| Boiling Point: | 333.09°C (rough estimate) |
| Flash Point: | 213.864oC |
| PSA: | 46.01000 |
| LogP: | 2.48860 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With water Flow reactor; | 90% |
| Stage #1: phenazine methosulfate With water for 58.5h; Irradiation; Inert atmosphere; Stage #2: With sodium hydroxide In water for 36h; Inert atmosphere; | 37% |
| Stage #1: phenazine methosulfate With water for 58.5h; Irradiation; Inert atmosphere; Stage #2: With sodium hydroxide In water for 36h; Inert atmosphere; | 37% |
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen bromide; acetic acid In water for 8h; Reflux; | 68% |
| With hydrogen bromide at 110 - 120℃; | |
| With hydrogen bromide; acetic acid | |
| With sodium methylate at 165℃; | |
| With boron tribromide In dichloromethane |
- 16101-29-4
1-acetoxy-1,2,3,4-tetrahydrophenazine-5-oxide
- 528-71-2
phenazin-1-ol
Conditions
| Conditions | Yield |
|---|---|
| With potassium hydroxide In methanol for 0.25h; Reflux; | 37% |
- 528-71-2
phenazin-1-ol
Conditions
| Conditions | Yield |
|---|---|
| With trifluoroacetic acid at 20℃; | 37% |
- 145657-29-0
3-(2-nitrophenylamino)-2-cyclohexen-1-one
- 528-71-2
phenazin-1-ol
Conditions
| Conditions | Yield |
|---|---|
| With carbon monoxide; 1,3-bis-(diphenylphosphino)propane; 1,10-phenanthroline hydrate; bis(dibenzylideneacetone)-palladium(0) In N,N-dimethyl-formamide at 120℃; under 4560.31 Torr; for 22h; | 26% |
Conditions
| Conditions | Yield |
|---|---|
| With phosphoric acid at 150 - 160℃; |
Conditions
| Conditions | Yield |
|---|---|
| With sodium methylate at 165℃; | |
| Multi-step reaction with 2 steps 1: methanol. sodium methylate / 140 °C 2: methanol. sodium methylate / 165 °C View Scheme |
- 860693-55-6
4-(2-amino-anilino)-3,5-dinitro-benzoic acid
A
- 2876-22-4
phenazin-1-ylamine
B
- 528-71-2
phenazin-1-ol
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; water; tin(ll) chloride und Erhitzen des Reaktionsgemisches mit wss.HCl; | |
| With hydrogenchloride; tin(ll) chloride Erhitzen des Reaktionsgemisches mit wss. HCl; |
- 15216-09-8, 392287-05-7
Anhydro [5-methyl-1-hydroxyphenazinium hydroxide]
- 528-71-2
phenazin-1-ol
- Total:19 Page 1 of 1 1
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