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Basic Information
| CAS No.: | 3677-81-4 |
|---|---|
| Name: | Borane, chlorodiphenyl- |
| Article Data: | 41 |
| Molecular Structure: | |
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|
|
| Formula: | C12H10BCl |
| Molecular Weight: | 200.475 |
| Synonyms: | diphenylchloroboron;BPh2Cl;chlorodiphenylborane;(c-Hex)2BCl;BClPh2;diphenyl boron chloride; |
| PSA: | 0.00000 |
| LogP: | 2.03110 |
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Synthetic route
- 7397-50-4
diphenyl(diethylamino)borane
- 10294-34-5
boron trichloride
A
- 3677-81-4
diphenylboronchloride
B
- 868-30-4
Diethylaminodichloroborane
Conditions
| Conditions | Yield |
|---|---|
| distn. of BCl3 into (C6H5)2BN(C2H5)2 at -50°C; distn.; | A 94% B n/a |
| distn. of BCl3 into (C6H5)2BN(C2H5)2 at -50°C; distn.; | A 94% B n/a |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With octene-1; Bis(borolane) In xylene introduction of BCl3 into soln. of B(C6H5)3 and bis(borolane), stirring at 120°C for 15 min (cooler at -78°C), addn. of octene-1; vac. distn; further product obtained by adding bis(borolane) to unified residue and predistillate and repeating procedure; | 77% |
Conditions
| Conditions | Yield |
|---|---|
| In benzene pouring BCl3 in soln. of Sn(C6H5)4 at 10°C, boiling under reflux (cooler at -78°C) for 3 h, with water temp. cooler for further 48 h; removing benzene by distn., twofold fractionated distn. of product at reduced pressure; | 75% |
| In benzene pouring BCl3 in soln. of Sn(C6H5)4 at 10°C, boiling under reflux (cooler at -78°C) for 3 h, with water temp. cooler for further 48 h; removing benzene by distn., twofold fractionated distn. of product at reduced pressure; | 75% |
Conditions
| Conditions | Yield |
|---|---|
| In n-heptane byproducts: dimethyltin dichloride; glovebox; addn. of 1 equiv. of BCl3 as 1 M soln. in heptane to a flask contg. dimethyldiaryltin and heptane at room temp., sealing, stirring at room temp. for 30 min, heating at 100°C in oil bath for 24-48 h; cooling, decantation, removal of volatiles, recrystn. from petroleum ether at -35°C; | 72.8% |
| In n-heptane |
Conditions
| Conditions | Yield |
|---|---|
| With phosphorus pentachloride at 150℃; Inert atmosphere; | 63% |
| With boron trichloride at -80℃; | |
| With phosphorus pentachloride |
- 15323-04-3
diphenylborinic acid butyl ester
- 3677-81-4
diphenylboronchloride
Conditions
| Conditions | Yield |
|---|---|
| With boron trichloride at -80℃; |
- 98882-69-0
diphenyl-propoxy-borane
- 3677-81-4
diphenylboronchloride
Conditions
| Conditions | Yield |
|---|---|
| With phosphorus pentachloride |
Conditions
| Conditions | Yield |
|---|---|
| at 300 - 320℃; extrahiert das Produkt mit Petrolaether; |
Conditions
| Conditions | Yield |
|---|---|
| With silver Irradiation; | |
| photolysis; |
Conditions
| Conditions | Yield |
|---|---|
| With di-n-butylborane; phenylborondichloride |
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Borane, chlorodiphenyl-
