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| CAS No.: | 2956-58-3 |
|---|---|
| Name: | N,N'-ETHYLENEBISACRYLAMIDE |
| Article Data: | 13 |
| Molecular Structure: | |
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|
|
| Formula: | C8H12N2O2 |
| Molecular Weight: | 168.195 |
| Synonyms: | Acrylamide,N,N'-ethylenebis- (6CI,7CI,8CI);Ethylenebisacrylamide;N,N'-Bisacryloylethylenediamine;N,N'-Diacryloyl-1,2-diaminoethane;N,N'-Ethylenebisacrylamide; |
| Density: | 1.034 g/cm3 |
| Melting Point: | 138-140 °C(lit.) |
| Boiling Point: | 456.3 °C at 760 mmHg |
| Flash Point: | 213 °C |
| Solubility: | Soluble in water and methanol. |
| Appearance: | WHITE TO OFF-WHITE TO FAINT RED POWDER,CRYSTALS OR CRYSTALLINE POWDER |
| Hazard Symbols: |
 Xi, Xn, F
|
| Risk Codes: | 36/37/38-40-11 |
| Safety: | 26-36/37/39-20 |
| PSA: | 58.20000 |
| LogP: | 0.37260 |
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- 68439-39-4Poly(oxy-1,2-ethanediyl), alpha-(2-ethylhexyl)-omega-hydroxy-,
- 852475-26-4MC1568
- 107-15-3
ethylenediamine
- 814-68-6
acryloyl chloride
A
- 2956-58-3
N,N'-ethylenebisacrylamide
B
- 333-18-6
1,2-diaminoethane dihydrochloride
| Conditions | Yield |
|---|---|
| In acetonitrile for 2h; Ambient temperature; | A 85% B n/a |
| Conditions | Yield |
|---|---|
| With sodium acetate; hydroquinone In chloroform for 1h; Heating; | 80% |
| With 4-methoxy-phenol In dichloromethane at 0 - 5℃; for 6h; | 56% |
| With sodium hydroxide In water; acetonitrile at 20℃; for 6h; Cooling with ice; | 40% |
| With sodium acetate In chloroform at 0 - 60℃; for 2.33h; | 36% |
| With triethylamine In chloroform |
| Conditions | Yield |
|---|---|
| With carbon monoxide; tetracarbonyl nickel; acetone |
- 2956-58-3
N,N'-ethylenebisacrylamide
| Conditions | Yield |
|---|---|
| With potassium hydroxide at 85 - 90℃; |
- 2680-03-7
N,N-Dimethylacrylamide
- 2956-58-3
N,N'-ethylenebisacrylamide
- polymer, reverse-phase suspension copolymerization, NH2 content 305 μmol/g; monomer(s): 2-methoxy-6-[(4-vinyl)benzyloxy]benzylamine hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide
polymer, reverse-phase suspension copolymerization, NH2 content 305 μmol/g; monomer(s): 2-methoxy-6-[(4-vinyl)benzyloxy]benzylamine hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide
| Conditions | Yield |
|---|---|
| With sorbitol tri-oleate; N,N,N,N,-tetramethylethylenediamine; adenosine 5'-phosphosulfate; N,N-dimethyl-formamide In tetrachloromethane; hexane; water at 35℃; for 120h; | 99% |
| Conditions | Yield |
|---|---|
| With PNODAM-5 catalyst In n-heptane; N,N-dimethyl acetamide at 100℃; Heck reaction; | 96% |
- 2680-03-7
N,N-Dimethylacrylamide
- 2956-58-3
N,N'-ethylenebisacrylamide
- polymer, reverse-phase suspension copolymerization, NH2 content 932 μmol/g; monomer(s): 4-(2-aminoethyl)styrene hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide
polymer, reverse-phase suspension copolymerization, NH2 content 932 μmol/g; monomer(s): 4-(2-aminoethyl)styrene hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide
| Conditions | Yield |
|---|---|
| With sorbitol tri-oleate; N,N,N,N,-tetramethylethylenediamine; adenosine 5'-phosphosulfate In tetrachloromethane; hexane; water at 35℃; for 1.75h; | 92% |
- 2680-03-7
N,N-Dimethylacrylamide
- 2956-58-3
N,N'-ethylenebisacrylamide
- polymer, reverse-phase suspension copolymerization, NH2 content 696 μmol/g; monomer(s): 4-aminomethylstyrene hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide
polymer, reverse-phase suspension copolymerization, NH2 content 696 μmol/g; monomer(s): 4-aminomethylstyrene hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide
| Conditions | Yield |
|---|---|
| With sorbitol tri-oleate; N,N,N,N,-tetramethylethylenediamine; adenosine 5'-phosphosulfate In tetrachloromethane; hexane; water at 35℃; for 1.5h; | 92% |
- 2680-03-7
N,N-Dimethylacrylamide
- 2956-58-3
N,N'-ethylenebisacrylamide
- polymer, reverse-phase suspension copolymerization, NH2 content 894 μmol/g; monomer(s): 4-(4-aminobutyl)styrene hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide
polymer, reverse-phase suspension copolymerization, NH2 content 894 μmol/g; monomer(s): 4-(4-aminobutyl)styrene hydrochloride; N,N-dimethylacrylamide; N,N-ethylenebisacrylamide
| Conditions | Yield |
|---|---|
| With sorbitol tri-oleate; N,N,N,N,-tetramethylethylenediamine; adenosine 5'-phosphosulfate In tetrachloromethane; hexane; water at 35℃; for 1.5h; | 92% |
| Conditions | Yield |
|---|---|
| With 2,4-di-tert-Butylphenol; toluene-4-sulfonic acid In chloroform Ambient temperature; 2-4d; | 82% |
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Specification
The 2-Propenamide,N,N'-1,2-ethanediylbis-, with the CAS registry number 2956-58-3, is also known as N,N'-Ethylenebis(acrylamide). It belongs to the product category of Anilines, Aromatic Amines and Nitro Compounds. This chemical's molecular formula is C8H12N2O2 and molecular weight is 168.19308. Its IUPAC name is called N-[2-(prop-2-enoylamino)ethyl]prop-2-enamide. The product should be sealed and stored in cool and dry place at temperature of 2-8 °C.
Physical properties of 2-Propenamide,N,N'-1,2-ethanediylbis-: (1)ACD/LogP: -1.28; (2)ACD/LogD (pH 5.5): -1.28; (3)ACD/LogD (pH 7.4): -1.28; (4)ACD/BCF (pH 5.5): 1; (5)ACD/BCF (pH 7.4): 1; (6)ACD/KOC (pH 5.5): 4.82; (7)ACD/KOC (pH 7.4): 4.82; (8)#H bond acceptors: 4; (9)#H bond donors: 2; (10)#Freely Rotating Bonds: 5; (11)Index of Refraction: 1.475; (12)Molar Refractivity: 45.81 cm3; (13)Molar Volume: 162.6 cm3; (14)Surface Tension: 34.6 dyne/cm; (15)Density: 1.034 g/cm3; (16)Flash Point: 213 °C; (17)Enthalpy of Vaporization: 71.63 kJ/mol; (18)Boiling Point: 456.3 °C at 760 mmHg; (19)Vapour Pressure: 1.63E-08 mmHg at 25°C.
Preparation: this chemical can be prepared by acryloyl chloride and ethane-1,2-diamine. This reaction will need reagent Et3N and solvent CHCl3.
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Uses of 2-Propenamide,N,N'-1,2-ethanediylbis-: it can be used to produce N,N'-Dicinnamoyl-ethylendiamin at temperature of 100 °C. This reaction is a kind of Heck reaction. It will need reagent PNODAM-5 catalyst and solvent heptane, N,N-dimethyl-acetamide. The yield is about 96%.
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When you are using this chemical, please be cautious about it as the following:
This chemical may cause inflammation to the skin or other mucous membranes. It is irritating to eyes, respiratory system and skin. In case of contact with eyes, you should rinse immediately with plenty of water and seek medical advice. Whenever you will contact it, please wear suitable protective clothing, gloves and eye/face protection.
You can still convert the following datas into molecular structure:
(1)Canonical SMILES: C=CC(=O)NCCNC(=O)C=C
(2)InChI: InChI=1S/C8H12N2O2/c1-3-7(11)9-5-6-10-8(12)4-2/h3-4H,1-2,5-6H2,(H,9,11)(H,10,12)
(3)InChIKey: AYGYHGXUJBFUJU-UHFFFAOYSA-N