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Basic Information
| CAS No.: | 22867-74-9 |
|---|---|
| Name: | 7-Ethylindole |
| Article Data: | 8 |
| Molecular Structure: | |
|
|
|
| Formula: | C10H11N |
| Molecular Weight: | 145.204 |
| Synonyms: | TIMTEC-BB SBB007573;7-ETHYLINDOLE;7-ETHYL-INDOL;7-ETHYLINDOLE(ETODOLAC INTERMEDIATE);7-Ethylindole,98+%;7-ETHYLCAMPTOTHECINSM-47-ETHYLINDOLE |
| EINECS: | -0 |
| Density: | 1.058 |
| Melting Point: | 230 ºC |
| Boiling Point: | 281.9 °C at 760 mmHg |
| Flash Point: | 119.9 °C |
| Solubility: | INSOLUBLE |
| Appearance: | Pale yellow clear liquid |
| Safety: | S23;S24/25 |
| PSA: | 15.79000 |
| LogP: | 2.73030 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With triphenylphosphine; tin(ll) chloride; ruthenium trichloride In 1,4-dioxane; water at 180℃; for 20h; Cyclization; | 87% |
| With tin(ll) chloride; ruthenium trichloride; triphenylphosphine In 1,4-dioxane; water at 180℃; for 20h; | 87% |
Conditions
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at -40℃; for 1h; Inert atmosphere; | 41% |
- 343791-43-5
1-(2-Amino-3-ethyl-phenyl)-2-chloro-ethanone
- 22867-74-9
7-ethyl-1H-indole
Conditions
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate In 1,4-dioxane; water for 1h; Heating; Yield given; |
Conditions
| Conditions | Yield |
|---|---|
| With silica gel; zirconium(IV) oxide at 309.85℃; | 54.2 % Chromat. |
- 578-54-1
ortho-ethylaniline
- 22867-74-9
7-ethyl-1H-indole
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 1.) BCl3, AlCl3, 2.) 2 N HCl / 1.) C6H6, CH2Cl2, reflux, 3 h, 2.) C6H6, CH2Cl2, 80 deg C, 45 min 2: NaBH4 / dioxane; H2O / 1 h / Heating View Scheme |
- 64-17-5
ethanol
- 109-89-7
diethylamine
- 108-90-7
chlorobenzene
- 98-83-9
isopropenylbenzene
- 22867-74-9
7-ethyl-1H-indole
Conditions
| Conditions | Yield |
|---|---|
| With triethylamine |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With potassium In triethylamine |
...Expand
- 22867-74-9
7-ethyl-1H-indole
- 24424-99-5
di-tert-butyl dicarbonate
- 396074-57-0
7-ethyl-1H-indole-1-carboxylic acid tert-butyl ester
Conditions
| Conditions | Yield |
|---|---|
| With dmap In acetonitrile | 100% |
| With dmap In acetonitrile | 100% |
| With dmap In acetonitrile at 20℃; for 3h; | 82% |
- 22867-74-9
7-ethyl-1H-indole
- 431-46-9
2,2,2-trifluoro-1-methoxy-ethanol
- 24313-88-0
3,4,5-Trimethoxyaniline
- 1132829-55-0
N-((R)-2,2,2-trifluoro-1-(7-ethyl-1H-indol-3-yl)ethyl)-3,4,5-trimethoxybenzenamine
Conditions
| Conditions | Yield |
|---|---|
| With (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In dichloromethane at 20℃; for 48h; Friedel Crafts aminoalkylation; Molecular sieve; optical yield given as %ee; enantioselective reaction; | 99% |
...Expand
- 22867-74-9
7-ethyl-1H-indole
- 434-45-7
1,1,1-trifluoroacetophenone
- 1160936-86-6
2,2,2-trifluoro-1-(7-ethyl-1H-indole-3-yl)-1-phenylethanol
Conditions
| Conditions | Yield |
|---|---|
| With (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In dichloromethane at 25℃; for 48h; optical yield given as %ee; enantioselective reaction; | 99% |
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7-Ethylindole
Chemistry
The molecular formula of 7-Ethylindole(22867-74-9) is C10H11N and its formula weight is 145.2.
The density of 7-Ethylindole(22867-74-9) is 1.058 g/mL at 20 °C(lit.) and it has a boiling point of 230 °C . The refractive index is about 1.603. Its flash point is 230°C.
The chemical synonyms of 7-Ethylindole(22867-74-9) are TIMTEC-BB SBB007573;7-ETHYLINDOLE;7-ETHYL-INDOL;7-ETHYLINDOLE(ETODOLAC INTERMEDIATE);7-Ethylindole,98+%;7-ETHYLCAMPTOTHECIN
The molecular structure of 7-Ethylindole(22867-74-9):
The density of 7-Ethylindole(22867-74-9) is 1.058 g/mL at 20 °C(lit.) and it has a boiling point of 230 °C . The refractive index is about 1.603. Its flash point is 230°C.
The chemical synonyms of 7-Ethylindole(22867-74-9) are TIMTEC-BB SBB007573;7-ETHYLINDOLE;7-ETHYL-INDOL;7-ETHYLINDOLE(ETODOLAC INTERMEDIATE);7-Ethylindole,98+%;7-ETHYLCAMPTOTHECIN
The molecular structure of 7-Ethylindole(22867-74-9):
Toxicity Data With Reference
RTECS#: CAS# 22867-74-9: None listed
LD50/LC50: RTECS: Not available.
Carcinogenicity: 7-ETHYLINDOLE, 97% - Not listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65.
LD50/LC50: RTECS: Not available.
Carcinogenicity: 7-ETHYLINDOLE, 97% - Not listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65.
Safety Profile
Safety Statements 23-24/25
WGK Germany 3
WGK Germany 3
Specification
Chemical Stability: Not available
Conditions to Avoid: Incompatible materials.
Incompatibilities with Other Materials Strong oxidizing agents.
Hazardous Decomposition Products Nitrogen oxides, carbon monoxide, carbon dioxide.
Hazardous Polymerization Has not been reported.
Conditions to Avoid: Incompatible materials.
Incompatibilities with Other Materials Strong oxidizing agents.
Hazardous Decomposition Products Nitrogen oxides, carbon monoxide, carbon dioxide.
Hazardous Polymerization Has not been reported.