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| CAS No.: | 15879-93-3 |
|---|---|
| Name: | alpha-Chloralose |
| Article Data: | 11 |
| Molecular Structure: | |
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|
|
| Formula: | C8H11Cl3O6 |
| Molecular Weight: | 309.531 |
| Synonyms: | Chloralose(6CI);Chloralose, a- (8CI);a-D-Glucofuranose,1,2-O-(2,2,2-trichloroethylidene)-, (R)-;AGC;AGC(carbohydrate);Alfa 4;Alpha 4;Alphakil;Anhydroglucochloral;Aphosal;Chloralosane;Dorcalm;Dulcidor;Glucochloral;Glucochloralose;Kalmettumsomniferum;Murex;Murex (carbohydrate);Somio;a-Chloralose;a-D-Chloralose;a-Monotrichloroethylidene-D-glucose; |
| EINECS: | 240-016-7 |
| Density: | 1.773 g/cm3 |
| Melting Point: | 178-182 °C |
| Boiling Point: | 504.4 °C at 760 mmHg |
| Flash Point: | 258.9 °C |
| Solubility: | 0.44 g/100 mL (15 °C) in water |
| Appearance: | needle-like crystals or powder |
| Hazard Symbols: |
 Xn
|
| Risk Codes: | 20/22 |
| Safety: | 16-24/25-28-28A |
| Transport Information: | UN 3249 |
| PSA: | 88.38000 |
| LogP: | -0.46290 |
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| Conditions | Yield |
|---|---|
| With sulfuric acid |
- 15879-93-3
α-chloralose
| Conditions | Yield |
|---|---|
| With methanol; sodium methylate |
- 39598-39-5
α-D-chloralose
- 15879-93-3
α-chloralose
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: pyridine 2: MeONa; MeOH View Scheme |
| Conditions | Yield |
|---|---|
| In chloroform |
- 15879-93-3
α-chloralose
| Conditions | Yield |
|---|---|
| With 4,4-dimethyl-5-methylene-1,3-dioxolan-2-one; 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 25℃; for 24h; | 90% |
- 77-76-9
2,2-dimethoxy-propane
- 15879-93-3
α-chloralose
| Conditions | Yield |
|---|---|
| With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 20℃; for 24h; | 84% |
| Conditions | Yield |
|---|---|
| With dmap In N,N-dimethyl-formamide at 25℃; for 24h; | 80% |
- 15879-93-3
α-chloralose
- 124595-32-0
(R)-1,2-O-(2,2,2-trichloroethylidene)-α-D-xylo-1,4-furanodialdose
| Conditions | Yield |
|---|---|
| With sodium periodate In methanol; water at 20℃; for 2h; | 78% |
| With sodium periodate In methanol; water at 20℃; for 4h; | 76% |
| With periodic acid | |
| With sodium periodate In methanol; water |
- 15879-93-3
α-chloralose
- 187029-11-4
1,2-O-R-(2,2,2-trichloroethylidene)-α-D-glucofuranose 3,5,6-phosphite
| Conditions | Yield |
|---|---|
| With hexaethylphosphorous triamide at 100 - 110℃; for 2h; | 74% |
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- Total:19 Page 1 of 1 1
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Chemistry
Chemical Name: alpha-Chloralose
IUPAC NAME: (1R)-1-[(2R,3aR,5R,6S,6aR)-6-Hydroxy-2-(trichloromethyl)-3a,5,6,6a-tetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethane-1,2-diol
CAS No.: 15879-93-3
EINECS: 240-016-7
RTECS: FM9450000
RTECS Class: Agricultural Chemical and Pesticide ; Tumorigen ; Human Data
EC Class: Harmful
Molecular Formula: C8H11Cl3O6
Molecular Weight: 309.53 g/mol
Melting Point: 178-182 °C
Density: 1.773 g/cm3
Flash Point: 258.9 °C
Boiling Point: 504.4 °C at 760 mmHg
Following is the structure of α-d-Glucochloralose (15879-93-3):
Product Categories about α-d-Glucochloralose (15879-93-3) are Biochemistry ; Glucose ; O-Substituted Sugars ; Sugars ; Dextrins、Sugar & Carbohydrates
The chemical synonymous of are (R)-1,2-O-(2,2,2-Trichloroethylidene)-alpha-D-glucofuranose ; 2-O-(2,2,2-Trichloroethylidene)-(R)-alpha-D-glucofuranos ; 2-O-(2,2,2-Trichloroethylidene)-(theta)-alpha-D-glucofuranos ; Alfamat ; Alpha-Chloralos ; Alphakil ; Aphosal ; Chloralosane
Toxicity Data With Reference
| 1. | orl-rat LDLo:400 mg/kg | 85ESA3 Merck Index; an Encyclopedia of Chemicals, Drugs, and Biologicals. 9 (1976),260. | ||
| 2. | scu-rat LDLo:200 mg/kg | 27ZIAQ Drug Dosages in Laboratory Animals-A Handbook C.D. Barnes andL.G. Eltherington,Berkeley, CA.: Univ. of California Press,1973,70. | ||
| 3. | orl-mus LD50:200 mg/kg | FMCHA2 Farm Chemicals Handbook .(Meister Publishing,Willoughy, OH.: )1991,C68. | ||
| 4. | ipr-mus LD50:175 mg/kg | ARZNAD Arzneimittel-Forschung. Drug Research. 21 (1971),1727. | ||
| 5. | orl-dog LD50:250 mg/kg | RMVEAG Recueil de Medecine Veterinaire. 154 (1978),137. | ||
| 6. | ipr-dog LDLo:400 mg/kg | AIPTAK Archives Internationales de Pharmacodynamie et de Therapie. 3 (1897),191. | ||
| 7. | orl-cat LD50:250 mg/kg | RMVEAG Recueil de Medecine Veterinaire. 154 (1978),137. | ||
| 8. | ipr-cat LDLo:150 mg/kg | AIPTAK Archives Internationales de Pharmacodynamie et de Therapie. 3 (1897),191. |
Consensus Reports
Reported in EPA TSCA Inventory.
Safety Profile
Poison by ingestion, subcutaneous, and intraperitoneal routes. Questionable carcinogen with experimental tumorigenic data. When heated to decomposition it emits toxic fumes of Cl−.
Hazard Codes:
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Risk Statements about α-d-Glucochloralose (15879-93-3):
R20/22 Harmful by inhalation and if swallowed.
Safety Statements about α-d-Glucochloralose (15879-93-3):
S16 Keep away from sources of ignition - No smoking.
S24/25 Avoid contact with skin and eyes.
S28A After contact with skin, wash immediately with plenty of water.
Attention:
1. Storage: Store in a cool, dry place. Store in a tightly closed container.
2. Handling: Wash thoroughly after handling. Use with adequate ventilation. Minimize dust generation and accumulation. Avoid contact with eyes, skin, and clothing. Do not ingest or inhale.