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Basic Information
CAS No.: 1533519-84-4
Name: 4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione
Article Data: 3
Molecular Structure:
Molecular Structure of 1533519-84-4 (4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione)
Formula: C15H13N3S
Molecular Weight: 267.354
Synonyms: 4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione;lesinurad int.4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione;4-(4-Cyclopropylnaphthalen-1-yl)-4H-1,2,4-triazole-3-thiol;Sodium 2-((4-(4-cyclopropylnaphthalen-1-yl)-4H-1,2,4-triazol-3-yl)thio)acetate;4-(4-cyclopropylnaphthalen-1-yl)-2,4-dihydro-3H-1,2,4-triazole-3-thione;Lesinurad Impurity 21;4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione (for Lesinurad)
EINECS: 943-285-5
Density: 1.41±0.1 g/cm3(Predicted)
Boiling Point: 435.2±38.0 °C(Predicted)
PSA: 69.51000
LogP: 3.58660
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Synthetic route
1533519-86-6

N-(4-cyclopropylnaphthalen-1-yl)-2-formylhydrazine-1-thiocarboxamide

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
With water; sodium hydroxide In N,N-dimethyl-formamide at 30℃; for 16h; Solvent; Temperature; Reagent/catalyst;90%
With potassium hydrogencarbonate In water; N,N-dimethyl-formamide at 90 - 140℃;

C12H8ClN3S

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cyclopropylmagnesium bromide

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
In tetrahydrofuran for 2h;89.89%
878671-94-4

1-amino-4-cyclopropylnaphthalene

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: water; 5,5-dimethyl-1,3-cyclohexadiene / 90 - 140 °C
2: N,N-dimethyl-formamide / 50 - 55 °C
3: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 4 steps
1: toluene; water
2: potassium hydroxide
3: N,N-dimethyl-formamide / 50 - 55 °C
4: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 3 steps
1.1: potassium carbonate / water; N,N-dimethyl-formamide / 3.5 h / 15 °C
1.2: 1 h / 0 °C
1.3: 2 h
2.1: ethyl acetate / 2 h / 60 °C
3.1: sodium hydroxide; water / N,N-dimethyl-formamide / 16 h / 30 °C
View Scheme
90-11-9

1-Bromonaphthalene

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 0 - 5 °C
2: nitric acid / 0 - 20 °C
3: palladium on activated charcoal; hydrogen
4: water; 5,5-dimethyl-1,3-cyclohexadiene / 90 - 140 °C
5: N,N-dimethyl-formamide / 50 - 55 °C
6: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 6 steps
1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 0 - 5 °C
2: nitric acid / 0 - 20 °C
3: hydrazine hydrate / methanol / Reflux
4: potassium hydroxide / dichloromethane
5: N,N-dimethyl-formamide / 50 - 55 °C
6: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 7 steps
1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 0 - 5 °C
2: nitric acid / 0 - 20 °C
3: palladium on activated charcoal; hydrogen
4: toluene; water
5: potassium hydroxide
6: N,N-dimethyl-formamide / 50 - 55 °C
7: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
25033-19-6

1-cyclopropyl-naphthalene

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: nitric acid / 0 - 20 °C
2: palladium on activated charcoal; hydrogen
3: water; 5,5-dimethyl-1,3-cyclohexadiene / 90 - 140 °C
4: N,N-dimethyl-formamide / 50 - 55 °C
5: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 5 steps
1: nitric acid / 0 - 20 °C
2: hydrazine hydrate / methanol / Reflux
3: potassium hydroxide / dichloromethane
4: N,N-dimethyl-formamide / 50 - 55 °C
5: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 6 steps
1: nitric acid / 0 - 20 °C
2: palladium on activated charcoal; hydrogen
3: toluene; water
4: potassium hydroxide
5: N,N-dimethyl-formamide / 50 - 55 °C
6: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
878671-93-3

1-cyclopropyl-4-nitronaphthalene

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: palladium on activated charcoal; hydrogen
2: water; 5,5-dimethyl-1,3-cyclohexadiene / 90 - 140 °C
3: N,N-dimethyl-formamide / 50 - 55 °C
4: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 4 steps
1: hydrazine hydrate / methanol / Reflux
2: potassium hydroxide / dichloromethane
3: N,N-dimethyl-formamide / 50 - 55 °C
4: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 5 steps
1: palladium on activated charcoal; hydrogen
2: toluene; water
3: potassium hydroxide
4: N,N-dimethyl-formamide / 50 - 55 °C
5: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
1533519-87-7

1-amino-4-cyclopropylnaphthalene oxalate

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: potassium hydroxide
2: N,N-dimethyl-formamide / 50 - 55 °C
3: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
878671-95-5

(1-cyclopropylnaphthalen-4-yl)isothiocyanate

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide / 50 - 55 °C
2: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 2 steps
1: ethyl acetate / 2 h / 60 °C
2: sodium hydroxide; water / N,N-dimethyl-formamide / 16 h / 30 °C
View Scheme
1533519-92-4

1-amino-4-cyclopropylnaphthalene hydrochloride

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: potassium hydroxide / dichloromethane
2: N,N-dimethyl-formamide / 50 - 55 °C
3: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
1533519-91-3

tert-butyl 4-cyclopropylnaphthalen-1-ylcarbamate

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: hydrogenchloride / ethanol
2: potassium hydroxide / dichloromethane
3: N,N-dimethyl-formamide / 50 - 55 °C
4: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
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    1533519-84-4

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  • 1533519-84-4 4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione

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    1533519-84-4

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    Product name: 4-(4-Cyclopropylnaphthalen-1-yl)-1H-1,2,4-Triazole-5(4H)-Thione CAS No.：1533519-84-4 Molecule Formula：C15H13N3S Molecule Weight：267.35 Purity: 98.0% Package: 25kg/drum Description：White or off-white powder Manufacture Standards：E

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    1533519-84-4

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    Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

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  • 4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thioneCAS NO.: 1533519-84-4

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    1533519-84-4

    4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thioneCAS NO.: 1533519-84-4

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  • Casno:

    1533519-84-4

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    Founded in 2008, East Chemsources Limited is a professional manufacturer of supplier in food and beverage, pharmaceuticals, cosmetics and other industries. pharmaceutical field in

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    1533519-84-4

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    Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

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  • Lesinurad Impurity 20

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    1533519-84-4

    Lesinurad Impurity 20

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    Business Type:Lab/Research institutions

    Tel:+86-173-20513646

    Address:Company address: Room 005, 15th Floor, Building D2, Phase III, Software New Town, No. 8 Huacheng Avenue, East Lake High-tech Development Zone, Wuhan, Hubei Province, China

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    1533519-84-4

    4-(4-Cyclopropylnaphthalen-1-yl)-4H-1,2,4-triazole-3-thiol

    Min.Order: 1 Metric Ton

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    1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

    KAISA GROUP INC.is the enterprise which is specialize in manfacturing and exporting avariety of Chemical in China. We have the strong economic base and comprehensive technology.We

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    United States  |  Contact Details

    Business Type:Trading Company

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  • 4-(4-cyclopropylnaphthalen-1-yl)-4h-1,2,4-triazole-3-thiol

  • Casno:

    1533519-84-4

    4-(4-cyclopropylnaphthalen-1-yl)-4h-1,2,4-triazole-3-thiol

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an

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     China (Mainland)  |  Contact Details

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    1533519-84-4

    4-(4-Cyclopropylnaphthalen-1-yl)-4H-1,2,4-triazole-3-thiol

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    High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

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  • Casno:

    1533519-84-4

    4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione

    Min.Order: 1 Kilogram

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    China (Mainland)  |  Contact Details

    Business Type:Other

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  • 1533519-84-4 LESINURAD INTERMEDIA / high quality /Best price/In stock

  • Casno:

    1533519-84-4

    1533519-84-4 LESINURAD INTERMEDIA / high quality /Best price/In stock

    Min.Order: 1 Metric Ton

    FOB Price:  USD $ 1.0-1.0

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    China (Mainland)  |  Contact Details

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