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Basic Information
CAS No.: 152828-25-6
Name: 2-(4-aminophenyl)-6-tert-butyl-1H-pyrazolo[1,5-b][1,2,4]triazole
Molecular Structure:
Molecular Structure of 152828-25-6 (2-(4-aminophenyl)-6-tert-butyl-1H-pyrazolo[1,5-b][1,2,4]triazole)
Formula: C14H17 N5
Molecular Weight: 255.322
Synonyms: Benzenamine,4-[6-(1,1-dimethylethyl)-1H-pyrazolo[1,5-b][1,2,4]triazol-2-yl]- (9CI);1H-Pyrazolo[1,5-b][1,2,4]triazole, benzenamine deriv.
Density: 1.29g/cm3
Hazard Symbols: Xi,N
PSA: 72.00000
LogP: 3.18530
Synthetic route
7795-95-1

octane-1-sulfonyl chloride

152828-25-6

C14H17N5

C22H33N5O2S

Conditions
ConditionsYield
With pyridine at 5 - 25℃; for 2h;91%
With pyridine at 5 - 25℃; for 2h;91%
2633-67-2

4-vinylbenzenesulfonyl chloride

152828-25-6

C14H17N5

C22H23N5O2S

Conditions
ConditionsYield
In tetrahydrofuran; ethyl acetate at 5 - 20℃; for 3h;91%
With picoline In tetrahydrofuran; ethyl acetate at 20℃; for 3h;91%
With picoline In tetrahydrofuran; ethyl acetate at 20℃; for 3h;91%
With picoline In tetrahydrofuran; ethyl acetate at 5 - 20℃; for 3h;91%
85-44-9

phthalic anhydride

152828-25-6

C14H17N5

1462320-85-9

C22H19N5O2

Conditions
ConditionsYield
In acetic acid at 120℃; for 3h;56g
152828-25-6

C14H17N5

1885-14-9

phenyl chloroformate

1462320-93-9

C21H21N5O2

Conditions
ConditionsYield
at 20℃; for 2h;50g
152828-25-6

C14H17N5

1462320-86-0

C45H36N10O4

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: acetic acid / 3 h / 120 °C
2: acetic anhydride / 2 h / 85 °C
View Scheme
152828-25-6

C14H17N5

1462320-89-3

C23H18ClN5O3

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: acetic acid / 3 h / 120 °C
2.1: trichlorophosphate / 1 h / 80 °C / Cooling with ice
2.2: 1 h / 80 °C
View Scheme
152828-25-6

C14H17N5

1462320-90-6

C29H25N9O2

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: acetic acid / 3 h / 120 °C
2.1: trichlorophosphate / 1 h / 80 °C / Cooling with ice
2.2: 1 h / 80 °C
3.1: pyridine / isopropyl alcohol / 6 h / Reflux
View Scheme
152828-25-6

C14H17N5

162208-37-9

C15H19N5O2S

Conditions
ConditionsYield
With methanesulfonyl chloride In pyridine at 20℃; for 2h;42g
152828-25-6

C14H17N5

1462320-92-8

C31H36N10O4S2

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: methanesulfonyl chloride / pyridine / 2 h / 20 °C
2: acetic acid / 2 h / 85 °C
View Scheme
152828-25-6

C14H17N5

1462320-84-8

C33H36N10O2

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: acetic acid / 2 h / 85 °C
2: acetic acid / 2 h / 85 °C
View Scheme
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    152828-25-6 CAS NO.152828-25-6

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