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Basic Information
CAS No.: 131276-24-9
Name: 1,8-Bis(diphenylphosphino)anthra
Article Data: 4
Molecular Structure:
Molecular Structure of 131276-24-9 (1,8-Bis(diphenylphosphino)anthra)
Formula: C14H8Br2
Molecular Weight: 336.026
Synonyms: 1,8-Bis(diphenylphosphino)anthra;1,8-Bis(diphenylphosphino)anthracene
Density: 1.768±0.06 g/cm3(Predicted)
Melting Point: 166.0 to 170.0 °C
Boiling Point: 438.8±18.0 °C(Predicted)
PSA: 0.00000
LogP: 0.00000
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Stage #2: With hydrogenchloride In methanol Heating;
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Conditions
ConditionsYield
Stage #1: 1,8-dibromo-10-anthrone With sodium tetrahydroborate In propan-1-ol
Stage #2: With hydrogenchloride		76%
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Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 62 percent / CuCl2; KBr; H3PO4 / nitrobenzene / Heating
2.1: sodium borohydride / methanol / -78 °C
2.2: HCl / methanol / Heating
2.3: 6.6 g / sodium borohydride / bis-(2-methoxy-ethyl) ether; methanol / 20 °C
View Scheme
Multi-step reaction with 2 steps
1.1: CuCl2; KBr; H3PO4 / nitrobenzene / Heating
2.1: sodium borohydride / methanol / -78 °C
2.2: HCl / methanol / Heating
2.3: 6.6 g / sodium borohydride / bis-(2-methoxy-ethyl) ether; methanol / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: potassium bromide; copper dichloride; phosphoric acid / nitrobenzene / 48 h / Reflux
2: aluminum isopropoxide; cyclohexanol / 72 h / Reflux
View Scheme
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1,8-dibromoanthraquinone

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p-benzoquinone

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Conditions
ConditionsYield
In isopropyl alcohol Schlenk technique; Inert atmosphere; Reflux;96%
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1,8-dibromoanthraquinone

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Conditions
ConditionsYield
With palladium diacetate; potassium carbonate; catacxium A In 1,2-dimethoxyethane; water at 85℃; for 20h; Suzuki-Miyaura Coupling; Inert atmosphere;95%
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Conditions
ConditionsYield
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Conditions
ConditionsYield
Stage #1: 1,8-dibromoanthraquinone With phenyllithium In tetrahydrofuran; dibutyl ether at -78℃; for 1.16667h; Inert atmosphere;
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Conditions
ConditionsYield
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Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water for 18h; Suzuki Coupling; Reflux;84%
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1,8-dibromoanthraquinone

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Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 90℃; for 14h; Inert atmosphere;83%
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    Business Type:Trading Company

    Tel:13165407087

    Address:Bock B, Yunshang Building, High-tech Zone

       Inquiry Now

  • OLED Intermediates 1,8-Bis(diphenylphosphino)anthra

  • Casno:

    131276-24-9

    OLED Intermediates 1,8-Bis(diphenylphosphino)anthra

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

    Our company has been engaged in the Pharmaceutical raw material and pharmaceutical intermediates medicine material intermediates and related chemical industry for more than ten ye

  • Taizhou volsen chemical Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-576-88869393

    Address:Jiaojiang District, Taizhou, Zhejiang, China.

       Inquiry Now

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