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Basic Information
| CAS No.: | 10591-84-1 |
|---|---|
| Name: | BIS(METHYLPHENYLTHIOCARBAMOYL)DISULFIDE |
| Molecular Structure: | |
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| Formula: | C16H16 N2 S4 |
| Molecular Weight: | 364.58 |
| Synonyms: | Disulfide,bis(methylphenylthiocarbamoyl) (6CI,7CI,8CI); Bis(methylphenylthiocarbamoyl)disulfide;N,N'-Dimethyl-N,N'-diphenylthiuram disulfide; NSC 37161; Vulkacit J; VulkaciteJ |
| Density: | 1.379g/cm3 |
| Melting Point: | 168-170 °C(Solv: ethanol (64-17-5)) |
| Boiling Point: | 478.3°Cat760mmHg |
| Flash Point: | 243.1°C |
| Solubility: | 10ng/L at 20℃ |
| PSA: | 121.26000 |
| LogP: | 5.21040 |
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Synthetic route
- 75-15-0
carbon disulfide
- 100-61-8
N-methylaniline
- 10591-84-1
N,N’-dimethyl-N,N’-diphenylthiuram disulfide
Conditions
| Conditions | Yield |
|---|---|
| With N,N-diethylnmethylamine; dihydrogen peroxide In toluene at 0 - 10℃; for 27.5h; Temperature; Reagent/catalyst; Solvent; Large scale; | 98.9% |
| With sodium hydroxide at 50℃; for 6h; | 75% |
| Stage #1: carbon disulfide; N-methylaniline With potassium hydroxide In tetrahydrofuran; water at 20℃; for 12h; Stage #2: With iodine In tetrahydrofuran; methanol; water at 20℃; for 1h; | 67% |
- 37600-51-4
methyl-phenyl-dithiocarbamic acid
- 10591-84-1
N,N’-dimethyl-N,N’-diphenylthiuram disulfide
Conditions
| Conditions | Yield |
|---|---|
| With air; nitrogen oxides in sodaalkolische Loesung; |
- 10591-84-1
N,N’-dimethyl-N,N’-diphenylthiuram disulfide
Conditions
| Conditions | Yield |
|---|---|
| With sodium sulfide; ethanol und Behandeln der mit Wasser versetzten Reaktionsloesung mit Bromcyan; |
Conditions
| Conditions | Yield |
|---|---|
| With ethanol; iodine durch Oxydation; oder mit einem anderen Oxydationsmittel; |
- 10591-84-1
N,N’-dimethyl-N,N’-diphenylthiuram disulfide
Conditions
| Conditions | Yield |
|---|---|
| With sodium trithionate; ethanol |
- 19009-45-1
N-methyl-N-phenylthiocarbamoyl chloride
- 10591-84-1
N,N’-dimethyl-N,N’-diphenylthiuram disulfide
- 100-61-8
N-methylaniline
- 10591-84-1
N,N’-dimethyl-N,N’-diphenylthiuram disulfide
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: diethyl ether View Scheme |
- 19009-45-1
N-methyl-N-phenylthiocarbamoyl chloride
- 10591-84-1
N,N’-dimethyl-N,N’-diphenylthiuram disulfide
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: ethanol 2: ethanol; sodium sulfide / und Behandeln der mit Wasser versetzten Reaktionsloesung mit Bromcyan View Scheme |
- 506-68-3
bromocyane
- 39234-21-4
sodium N-methyl-N-phenyldithiocarbamate
- 10591-84-1
N,N’-dimethyl-N,N’-diphenylthiuram disulfide
Conditions
| Conditions | Yield |
|---|---|
| With potassium iodide In water pH:6.2-6.7; in aqueous and non aqueous medium; titration method; |
- 83559-31-3
potassium N-methyl-N-phenyl-dithiocarbamate
- 10591-84-1
N,N’-dimethyl-N,N’-diphenylthiuram disulfide
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; sodium nitrite In methanol; water at 0 - 5℃; |
