Technology Process of Boron,(N-ethylethanamine)trihydro-, (T-4)-
There total 19 articles about Boron,(N-ethylethanamine)trihydro-, (T-4)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diethylamine;
In
acetone;
to NaBH4 in a flask is added a mixt. of acetonitrile and Et2NH, then slowly sulfur is added (15 h, 45°C); amine and acetone are removed, elem. anal.;
- Guidance literature:
-
With
water; sodium hydrogencarbonate;
In
tetrahydrofuran;
at 20 ℃;
for 4h;
DOI:10.1039/c6cc06031e