Benzamide, 3-amino-N-(3-aminophenyl)-

Base Information

• Chemical Name: Benzamide, 3-amino-N-(3-aminophenyl)-
• CAS No.: 101-12-2
• Deprecated CAS: 1036386-71-6
• Molecular Formula: C13H13 N3 O
• Molecular Weight: 227.266
• Hs Code.: 2924299090
• European Community (EC) Number: 202-917-3
• NSC Number: 13968
• DSSTox Substance ID: DTXSID7059226
• Nikkaji Number: J182.141E
• Wikidata: Q81988696
• Mol file: 101-12-2.mol

Synonyms:101-12-2;3,3'-Diaminobenzanilide;3-amino-n-(3-aminophenyl)benzamide;Benzamide, 3-amino-N-(3-aminophenyl)-;3-Amino-N-(3-amino-phenyl)-benzamide;3,3/'-Diaminobenzanilide;EINECS 202-917-3;NSC 13968;3,3'-diaminobenzanilid;NSC13968;Benzanilide,3'-diamino-;Oprea1_160787;CBDivE_013429;Benzanilide, 3,3'-diamino-;SCHEMBL308208;DTXSID7059226;NSC-13968;AKOS001483393;SR-01000389431;SR-01000389431-1

Chemical Property of Benzamide, 3-amino-N-(3-aminophenyl)-

Chemical Property:

• Boiling Point: 386.6oC at 760 mmHg
• Flash Point: 187.6oC
• PSA: 81.14000
• Density: 1.314g/cm3
• LogP: 3.33870
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 227.105862047
• Heavy Atom Count: 17
• Complexity: 269

Purity/Quality:

98%,99%, ^*data from raw suppliers

3-Amino-N-(3-amino-phenyl)-benzamide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)N)C(=O)NC2=CC=CC(=C2)N

Technology Process of Benzamide, 3-amino-N-(3-aminophenyl)-

There total 2 articles about Benzamide, 3-amino-N-(3-aminophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(3-nitrophenyl)-3-nitrobenzamide (101-24-6) → 3,3'-Diaminobenzanilide (101-12-2)

Guidance literature:

With ammonium sulfide;

Reference yield:

→ 3,3'-Diaminobenzanilide (101-12-2)

Guidance literature:

3,3'-Dinitrobenzanilid, SnCl2, HCl;

Reference yield:

3,3'-Diaminobenzanilide (101-12-2) + Ethyl oxalyl chloride (4755-77-5) → 3'-[m-(1-carboxyformamido)benzamido]-oxanilic acid (65481-33-6)

Guidance literature:

With triethylamine; In N-methyl-acetamide; water; ethyl acetate;

upstream raw materials:

N-(3-nitrophenyl)-3-nitrobenzamide

Downstream raw materials:

3'-[m-(1-carboxyformamido)benzamido]-oxanilic acid

Refernces

• 1、 -. "Anti-allergic oxanilate compounds". . . Retrieved 2008/06/13.