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Cas Database |
| Name |
Dichloro(1,5-cyclooctadiene)palladium(ii) |
EINECS | 235-161-8 |
| CAS No. | 12107-56-1 | Density | N/A |
| PSA | 0.00000 | LogP | 4.05180 |
| Solubility | insoluble in water | Melting Point |
210 °C (dec.)(lit.) |
| Formula | C8H12Cl2Pd | Boiling Point | 153.5 °C at 760 mmHg |
| Molecular Weight | 285.509 | Flash Point | 31.7 °C |
| Transport Information | N/A | Appearance | brown-black crystals |
| Safety | 26-37/39 | Risk Codes | 36/37/38 |
| Molecular Structure |
|
Hazard Symbols |
 Xi
|
| Synonyms |
Palladium,dichloro(1,5-cyclooctadiene)- (6CI,7CI,8CI);1,5-Cyclooctadiene, palladiumcomplex;(1,5-Cyclooctadiene)palladium dichloride;Dichloro(1,5-cyclooctadiene)palladium;Dichloro(cyclooctadiene)palladium;Dichloro(h4-1,5-cyclooctadiene)palladium;Dichloro[(1,2,5,6-h)-1,5-cyclooctadiene]palladium;NSC 169973; |
Article Data | 20 |
Dichloro(1,5-cyclooctadiene)palladium(ii) Synthetic route
- 1552-12-1, 111-78-4
1,5-cis,cis-cyclooctadiene
- 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)
| Conditions | Yield |
|---|---|
| Stage #1: palladium dichloride With hydrogenchloride In water Inert atmosphere; Schlenk technique; Stage #2: 1,5-cis,cis-cyclooctadiene In ethanol; water Inert atmosphere; Schlenk technique; | 98% |
| Stage #1: palladium dichloride With hydrogenchloride In ethanol Stage #2: 1,5-cis,cis-cyclooctadiene In ethanol |
- 5259-72-3, 10060-40-9, 111-78-4
1,5-dicyclooctadiene
- 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)
| Conditions | Yield |
|---|---|
| In hydrogenchloride; ethanol for 0.333333h; liquid HCl; | 96% |
| In methanol suspn. of PdCl2 (28.2 mmol) in MeOH reacted with COD (84.6 mmol) for 48 h at room temp. with stirring; filtered off, washed (MeOH), vacuum-dried; | 91% |
| In methanol at 20℃; for 48h; | 84% |
| With hydrogenchloride In water |
- 7647-01-0
hydrogenchloride
- 5259-72-3, 10060-40-9, 111-78-4
1,5-dicyclooctadiene
- 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)
| Conditions | Yield |
|---|---|
| Stage #1: hydrogenchloride; palladium dichloride at 20℃; Inert atmosphere; Stage #2: cyclo-octa-1,5-diene for 0.333333h; Inert atmosphere; | 95% |
- 7647-14-5
sodium chloride
- 5259-72-3, 10060-40-9, 111-78-4
1,5-dicyclooctadiene
- 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)
| Conditions | Yield |
|---|---|
| In methanol for 19h; | 93% |
- 865-49-6
chloroform-d1
- 5259-72-3, 10060-40-9, 111-78-4
1,5-dicyclooctadiene
- 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)
- 1042309-89-6
[Pd(acetonyl)Cl(1,5-cyclooctadiene)]
| Conditions | Yield |
|---|---|
| In acetone under N2; cyclooctadiene added to suspn. of Pd complex in acetone; detd. by (1)H NMR spectra in CDCl3; |
- 1042309-89-6
[Pd(acetonyl)Cl(1,5-cyclooctadiene)]
- 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)
| Conditions | Yield |
|---|---|
| In not given slowly decompd. in chlorinated solvents; |
- 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)
- 1425562-48-6
1-[N,N’,N’’-trimethyl-(4-butyl)ammonium]-4-(2-pyridyl)-1H-1,2,3-triazolechloride
- 1425725-67-2
[palladium(II) 1-(4-N,N’,N’’-trimethylbutylammonium)-4-(2-pyridyl)-1H-1,2,3-triazoledichloride]chloride
| Conditions | Yield |
|---|---|
| In methanol; dichloromethane for 1h; | 100% |
- 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)
- 13954-38-6
tripiperidino-phosphine
- 68494-72-4, 955117-31-4
dichloro{bis[1,1’,1’’-(phosphinetriyl)tripiperidine]}palladium(II)
| Conditions | Yield |
|---|---|
| In toluene at 20℃; for 0.166667h; | 100% |
- 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)
- 13170-43-9
(trimethylsilyl)methylmagnesium chloride
- 225931-80-6
bis[(trimethylsilyl)methyl](1,5-cyclooctadiene)palladium(II)
| Conditions | Yield |
|---|---|
| In diethyl ether at -25℃; for 1.5h; Inert atmosphere; | 100% |
| In diethyl ether at 0℃; for 0.5h; Inert atmosphere; | 72% |
| In diethyl ether at 0℃; for 0.333333h; Inert atmosphere; | 65% |
- 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)
| Conditions | Yield |
|---|---|
| In dichloromethane at 20℃; for 1h; Inert atmosphere; Schlenk technique; | 100% |
Dichloro(1,5-cyclooctadiene)palladium(ii) Chemical Properties
Chemical Name: Dichloro(1,5-cyclooctadiene)palladium(ii)
IUPAC NAME: (1Z,5Z)-cycloocta-1,5-diene,palladium(2+),dichloride
CAS No.: 12107-56-1
EINECS: 235-161-8
Molecular Formula: C8H12Cl2Pd
Formula Weight: 285.51 g/mol
Melting Point: 210 °C (dec.)(lit.)
Flash Point: 31.7 °C
Boiling Point: 153.5 °C at 760 mmHg
Sensitive: Hygroscopic
Following is the structure of Dichloro(1,5-cyclooctadiene)palladium(ii) (12107-56-1):
Product Categories about Dichloro(1,5-cyclooctadiene)palladium(ii) (12107-56-1) are Catalysts for Organic Synthesis ; Classes of Metal Compounds ; Homogeneous Catalysts ; Metal Complexes ; Pd (Palladium) Compounds ; Synthetic Organic Chemistry ; Transition Metal Compounds ; Catalysis and Inorganic Chemistry ; Homogeneous Pd Catalysts ; Palladium
The chemical synonymous of Dichloro(1,5-cyclooctadiene)palladium(ii) (12107-56-1) are Dichloro[(1,2,5,6-eta)-1,5-cyclooctadiene]-palladiu ; (1,5-Cyclooctadiene)palladium(ii)chloride ; 1,5-Cyclooctadienepalladium(ii) dichloride ; Dichloro(cycloocta-1,5-diene)palladium(ii) ; Dichloro(eta-cycloocta-1,5-diene)palladium (ii) ; Dichloro(1,5-cyclooctyldiene)palladium(ii)
Dichloro(1,5-cyclooctadiene)palladium(ii) Safety Profile
Hazard Codes:
Xi: Irritant .gif){kind=small}
Risk Statements about Dichloro(1,5-cyclooctadiene)palladium(ii) (12107-56-1):
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements about Dichloro(1,5-cyclooctadiene)palladium(ii) (12107-56-1):
S26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S37/39: Wear suitable gloves and eye/face protection.
Attentions:
1. Storage: Store in a cool, dry place. Store in a tightly closed container.
2. Handling: Avoid breathing dust, vapor, mist, or gas. Avoid contact with skin and eyes.
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