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Cytidine 5'-monophosphate disodium salt

  • Name Cytidine 5'-monophosphate disodium salt
  • EINECS229-819-3
  • CAS No. 6757-06-8
  • Density2.15g/cm3
  • PSA192.83000
  • LogP-0.98840
  • SolubilityN/A
  • Melting Point300 °C
  • FormulaC9H12N3Na2O8P
  • Boiling Point678.1oC at 760 mmHg
  • Molecular Weight367.163
  • Flash Point363.9oC
  • Transport InformationN/A
  • AppearanceWhite crystalline powder
  • Safety24/25
  • Risk Codes20/21/22-36/37/38
  • Molecular Structure
    Molecular Structure of 6757-06-8 (Cytidine 5'-monophosphate disodium salt)
  • Hazard SymbolsXn,Xi
  • SynonymsXn,Xi
  • Article Data1

Cytidine 5'-monophosphate disodium salt Synthetic route

C9H14N4O10P2(2-)*2Na(1+)

6757-06-8

cytidine-5'-monophosphate disodium salt

Conditions
ConditionsYield
With water; zinc(II) cation pH=5.5;
66-71-7

1,10-Phenanthroline

copper(II) nitrate hexahydrate

6757-06-8

cytidine-5'-monophosphate disodium salt

[Cu7(1,10-phenanthroline)6(cytidine 5'-monophosphate)4]*(NO3)6*(H2O)46

Conditions
ConditionsYield
In ethanol at 40℃;76%

Cu(NO3)2*2(ethylenediamine)

6757-06-8

cytidine-5'-monophosphate disodium salt

[Cu2(ethylenediamine)2(cytidine 5'-monophosphate)2]*5H2O

Conditions
ConditionsYield
In methanol for 0.5h; pH=4;75%

cobalt(II) nitrate hexahydrate

6757-06-8

cytidine-5'-monophosphate disodium salt

1135-32-6

trans-1,2-bis(4-pyridyl)ethylene

[Co(HCMP)2(bis(4-pyridyl)ethylene)(H2O)2]·3.5H2O

Conditions
ConditionsYield
Stage #1: cobalt(II) nitrate hexahydrate; cytidine-5'-monophosphate disodium salt; water for 0.5h;
Stage #2: trans-1,2-bis(4-pyridyl)ethylene With nitric acid In ethanol at 20℃; for 0.5h; pH=5;
72%

manganese(II) perchlorate hexahydrate

6757-06-8

cytidine-5'-monophosphate disodium salt

1135-32-6

trans-1,2-bis(4-pyridyl)ethylene

[Mn(bis(4-pyridyl)ethylene)(H2O)4]·(CMP)·3H2O

Conditions
ConditionsYield
Stage #1: manganese(II) perchlorate hexahydrate; cytidine-5'-monophosphate disodium salt; water for 0.5h;
Stage #2: trans-1,2-bis(4-pyridyl)ethylene With sodium hydroxide In ethanol at 20℃; for 0.5h; pH=6;
68%

manganese(II) perchlorate hexahydrate

6757-06-8

cytidine-5'-monophosphate disodium salt

1135-32-6

trans-1,2-bis(4-pyridyl)ethylene

[Mn(bis(4-pyridyl)ethylene)3(H2O)2]·(ClO4)2·(bis(4-pyridyl)ethylene)2·5H2O

Conditions
ConditionsYield
Stage #1: manganese(II) perchlorate hexahydrate; cytidine-5'-monophosphate disodium salt; water for 0.5h;
Stage #2: trans-1,2-bis(4-pyridyl)ethylene With sodium hydroxide In ethanol at 20℃; for 0.5h; pH=7;
68%
6757-06-8

cytidine-5'-monophosphate disodium salt

Conditions
ConditionsYield
With 3-chloro-benzenecarboperoxoic acid In methanol at 0 - 20℃; for 24.25h;42%

chromium(III)(L-ser)2(H2O)2Cl*H2O

6757-06-8

cytidine-5'-monophosphate disodium salt

(chromium(III))2(L-ser)2(5'-CMP)(OH)Cl*7H2O

Conditions
ConditionsYield
In water soln. of nucleotide (pH=7) is added dropwise to a soln. of amino acid chromium complex, soln. is placed in a thermostated bath at 50°C with const. stirring for 8 h; soln. is concd. to 5 ml, chromy. (Sephadex), addn. of ethanol to the first (blue) fraction, further evapn., ppt. is vac. dried (P4O10); elem. anal.;

chromium(III)(L-met)(L-metH)Cl2*3H2O

6757-06-8

cytidine-5'-monophosphate disodium salt

(chromium(III))2(L-met)(5'-CMP)2(OH)*10H2O

Conditions
ConditionsYield
In water soln. of nucleotide (pH approx. 7) is added dropwise to a soln. of amino acid chromium complex (pH 3.9-4.2), mixt. is maintained at 50°C with const. stirring for 1.5-2.5 h; ppt. is filtered off, washed with cold water and vac. dried (P4O10); elem. anal.;
6757-06-8

cytidine-5'-monophosphate disodium salt

Cr(3+)*NH2CH2CH2NH2*CONC(NH2)CHCHN(CHCHOHCHOHCH(CH2OPO3)O)(2-)*CONC(NH2)CHCHN(CHCHOHCHOHCH(CH2OPO3H)O)(1-)*8H2O

Conditions
ConditionsYield
In water aq. soln. of Cr compd. mixed with aq. soln. of org. compd. (mole ratio Cr : org. compd. = 1 : 1); soln. heated at ca. 55 °C for 5-7 h; soln. concd. at 50 °C and passed through a colomn; ethanol addedto eluate; resulting ppt. filtered, washed (EtOH), and dried over silica gel; elem. anal.;

Cytidine 5'-monophosphate disodium salt Chemical Properties

Molecular Structure of Cytidine 5'-monophosphate disodium salt (CAS NO.6757-06-8):

IUPAC Name: disodium [(2R,3S,4R,5R)-5-(4-amino-2-oxopyrimidin-1-yl)-3,4-dihydroxyoxolan-2-yl]methyl phosphate 
Empirical Formula: C9H12N3Na2O8P
Molecular Weight: 367.1602
H bond acceptors: 11
H bond donors: 4
Freely Rotating Bonds: 10
Polar Surface Area: 162.95Å2
EINECS: 229-819-3
Melting point: 300 °C
Product Categories: Amino Acids;Biochemistry;Nucleosides, Nucleotides & Related Reagents;Nucleotides and their analogs;Nucleic acids
InChI
InChI=1/C9H14N3O8P.2Na/c10-5-1-2-12(9(15)11-5)8-7(14)6(13)4(20-8)3-19-21(16,17)18;;/h1-2,4,6-8,13-14H,3H2,(H2,10,11,15)(H2,16,17,18);;/q;2*+1/p-2/t4-,6-,7-,8-;;/m1../s1
Smiles
n1([C@H]2[C@@H]([C@H](O)[C@H](O2)COP(=O)([O-])[O-])O)c(nc(cc1)N)=O.[Na+].[Na+]

Cytidine 5'-monophosphate disodium salt Safety Profile

Hazard Codes: HarmfulXn,IrritantXi
Risk Statements: 20/21/22-36/37/38
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed. 
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 22-24/25-37/39-36-26
S22:Do not breathe dust. 
S24/25:Avoid contact with skin and eyes. 
S37/39:Wear suitable gloves and eye/face protection. 
S36:Wear suitable protective clothing. 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
WGK Germany: 3
F: 1-10

Cytidine 5'-monophosphate disodium salt Specification

  Cytidine 5'-monophosphate disodium salt , with CAS number of 6757-06-8, can be called 5'-CMP disodium salt ; CMP disodium salt ; Cytidine 5'MP, disodium salt ; Cytidine monophosphate disodium salt ; Disodium 5'-CMP ; Disodium CMP ; Disodium cytidine 5'-monophosphate ; Disodium cytidine 5'-phosphate . It is a white crystalline powder.

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