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4-Chlorophenylhydrazine hydrochloride
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Name

4-Chlorophenylhydrazine hydrochloride

 EINECS 214-030-9
CAS No. 1073-70-7 Density 1.32 g/cm3
PSA 38.05000 LogP 3.20090
Solubility Soluble in hot water, methanol. Melting Point 216 °C (dec.)(lit.)
Formula C6H7ClN2.HCl Boiling Point 265.3 °C at 760 mmHg
Molecular Weight 179.049 Flash Point 114.2 °C
Transport Information 2811 Appearance white to pink crystalline powder
Safety 36/37-36-26 Risk Codes 20/21/22-36/37/38
Molecular Structure Molecular Structure of 1073-70-7 (4-Chlorophenylhydrazine hydrochloride) Hazard Symbols HarmfulXn,IrritantXi
Synonyms

P-Chloropheyl hydrazine HCl;Hydrazine,(4-chlorophenyl)-, monohydrochloride (9CI);Hydrazine, (p-chlorophenyl)-,monohydrochloride (8CI);4-Chlorophenylhydrazine hydrochloride;4-Chlorophenylhydrazine monohydrochloride;p-Chlorophenylhydrazinehydrochloride;p-Chlorophenylhydrazine monohydrochloride;

Article Data 38

4-Chlorophenylhydrazine hydrochloride Synthetic route

2028-74-2

p-chlorobenzenediazonium chloride

1073-70-7

4-chlorophenylhydrazine hydrochloride

Conditions
ConditionsYield
With 5% active carbon-supported ruthenium; hydrogen at 30℃; under 3750.38 Torr; for 4h; Temperature; Pressure; Reagent/catalyst;98.2%
With palladium on activated charcoal; hydrogen In water at 10℃; under 22502.3 Torr; Pressure; Temperature; Solvent; Reagent/catalyst;89.7%
829-31-2

3-(4-chlorophenyl)sydnone

1073-70-7

4-chlorophenylhydrazine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In ethyl acetate at 60℃; for 0.25h; Ring cleavage;90%
106-47-8

4-chloro-aniline

1073-70-7

4-chlorophenylhydrazine hydrochloride

Conditions
ConditionsYield
Stage #1: 4-chloro-aniline With hydrogenchloride; sodium nitrite In water for 1h;
Stage #2: With sodium sulfite at 80℃; for 2.5h;
Stage #3: With hydrogenchloride In water at 95℃; for 2h;		88.3%
Stage #1: 4-chloro-aniline With hydrogenchloride; sodium nitrite In water at 5℃;
Stage #2: With sodium carbonate; sodium sulfite In water at 5 - 70℃;		65.4%
Stage #1: 4-chloro-aniline With hydrogenchloride; sodium nitrite
Stage #2: With tin(ll) chloride		64.3%
106-39-8

bromochlorobenzene

1073-70-7

4-chlorophenylhydrazine hydrochloride

Conditions
ConditionsYield
Stage #1: bromochlorobenzene With hydrazine hydrate; copper(II) sulfate; cobalt(II) chloride In propylene glycol at 152℃; for 10h;
Stage #2: With hydrogenchloride In water Reagent/catalyst; Temperature; Solvent;		88.1%
Stage #1: bromochlorobenzene With 2,3,5,6,8,9,11,12,14,15-decahydro-1,4,7,10,13,16-benzohexaoxacyclooctadecin; hydrazine hydrate; copper(I) bromide In propylene glycol; water at 172℃; for 5h;
Stage #2: With hydrogenchloride In water at 70℃; pH=1.8; Reagent/catalyst; Solvent; Temperature; Time; pH-value;		86.3%
Stage #1: bromochlorobenzene With potassium phosphate; copper(l) iodide; N,N′-bis(2,6-dimethylphenyl)oxalamide; cetyltrimethylammonim bromide In water at 80℃; for 0.25h; Schlenk technique; Inert atmosphere; Sealed tube;
Stage #2: With hydrazine hydrate In water at 80℃; Inert atmosphere; Schlenk technique; Sealed tube;
Stage #3: With hydrogenchloride In water pH=3 - 4; Inert atmosphere; Schlenk technique; Sealed tube;		85%
Stage #1: bromochlorobenzene With potassium phosphate; N,N'-bis(2,5-dimethylpyrrol-1-yl)oxalamide; cetyltrimethylammonim bromide; copper(I) bromide In water at 110℃; for 0.166667h; Sealed tube; Inert atmosphere;
Stage #2: With hydrazine hydrate In water at 110℃; for 1.5h; Sealed tube; Inert atmosphere;
Stage #3: With hydrogenchloride In dichloromethane; water		80%
64-17-5

ethanol

54624-61-2

4-chloro-3-(4-chlorophenyl)sydnone

A

1073-70-7

4-chlorophenylhydrazine hydrochloride

B

N-(4-Chloro-phenyl)-hydrazinecarboxylic acid ethyl ester; hydrochloride

Conditions
ConditionsYield
With hydrogenchloride
1352877-23-6

(3R,4S)-4-hydroxy-2-oxotetrahydrofuran-3-yl 2-(2-(4-chlorophenyl)hydrazinyl)-2-oxoacetate

1073-70-7

4-chlorophenylhydrazine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In 1,4-dioxane; methanol at 90℃; for 2h;
36966-92-4

4-Chlor-phenylnitrosamin

1073-70-7

4-chlorophenylhydrazine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; tin(ll) chloride In water at 0℃;
563-80-4

3-methyl-butan-2-one

1073-70-7

4-chlorophenylhydrazine hydrochloride

25981-83-3

5-chloro-2,3,3-trimethyl-3H-indole

Conditions
ConditionsYield
With sulfuric acid In water at 100℃; for 0.166667h; Reagent/catalyst; Temperature; Microwave irradiation; Green chemistry;100%
With sulfuric acid In water at 100℃; for 0.166667h; Wavelength; Microwave irradiation; Inert atmosphere; Green chemistry;100%
With perchloric acid In ethanol Fischer indolization; Heating;88%
832-10-0

cyclotridecanone

1073-70-7

4-chlorophenylhydrazine hydrochloride

16-chloro-20-aza-tricyclo[11.7.0.014,19]eicosa-1(13),14(19),15,17-tetraene

Conditions
ConditionsYield
at 250℃; for 0.0166667h; Fischer indole synthesis;100%
1073-70-7

4-chlorophenylhydrazine hydrochloride

120-92-3

cyclopentanone

302912-35-2

7-chloro-1,2,3,4-tetrahydrocyclopenta[b]indole

Conditions
ConditionsYield
at 250℃; for 0.0166667h; Fischer indole synthesis;100%
With acetic acid Fischer Indole Synthesis; Reflux;10%

4-Chlorophenylhydrazine hydrochloride Chemical Properties

Product Name: 4-Chlorophenylhydrazine hydrochloride
Synonyms: P-CHLOROPHENYLHYDRAZINE HCL;4-CHLOROPHENYLHYDRAZINE HCL;4-CHLOROPHENYLHYDRAZINE HYDROCHLORIDE;LABOTEST-BB LT01147712; P-Chlorophenyluhydrazinehydrochloride;P-CHLOROPHENYLHYDRAZINE HYDROCHLORIDE;1-(4-CHLOROPHENYL)HYDRAZINE HYDROCHLORIDE;CHLOROPHENYLHYDRAZINE(4-) HCL;
The Molecular formula of p-Chlorophenylhydrazine HCl(1073-70-7): C6H8Cl2N2
The Molecular Weight of p-Chlorophenylhydrazine HCl(1073-70-7): 179.05
Molecular Structure : 
EINECS: 214-030-9
Melting point: 216 °C (dec.)(lit.)

4-Chlorophenylhydrazine hydrochloride Uses

p-Chlorophenylhydrazine HCl(1073-70-7) is used for synthetic organic intermediates.

4-Chlorophenylhydrazine hydrochloride Safety Profile

The Hazard Codes of p-Chlorophenylhydrazine HCl(1073-70-7) :   Xn,Xi
The Risk Statements information of p-Chlorophenylhydrazine HCl(1073-70-7):
20/21/22:  Harmful by inhalation, in contact with skin and if swallowed
36/37/38:  Irritating to eyes, respiratory system and skin 
The Safety Statements information of p-Chlorophenylhydrazine HCl(1073-70-7):
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
36:  Wear suitable protective clothing 
36/37:  Wear suitable protective clothing and gloves 
Hazard Note: Harmful/Irritant
HazardClass: 6.1(b)
HS Code: 29280090
PackingGroup: III
RIDADR: 2811
WGK Germany: 3

4-Chlorophenylhydrazine hydrochloride Analytical Methods

Liquid chromatographic analysis method.
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