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74563-64-7

Basic Information
CAS No.: 74563-64-7
Name: PHYTANTRIOL
Article Data: 3
Molecular Structure:
Molecular Structure of 74563-64-7 (PHYTANTRIOL)
Formula: C20H42 O3
Molecular Weight: 330.552
Synonyms: Phytanetriol;Phytantriol
Density: 0.932 g/mL at 25oC(lit.)
Melting Point: 56-57°
Boiling Point: 130oC0.01 mm Hg(lit.)
Flash Point: 199oC
Solubility: 352μg/L at 20℃
Safety:
WGK Germany 3
10
PSA: 60.69000
LogP: 4.52970
Synthetic route
105873-65-2

6,10,14-Trimethyl-2-(2-phenyl-[1,3]dioxolan-4-yl)-pentadecan-2-ol

74563-64-7

3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane

Conditions
ConditionsYield
With hydrogen; toluene-4-sulfonic acid; palladium In ethanol78%
7437-61-8

2-methyl-3,4-epoxy-1-butene

74563-64-7

3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 72 percent / tetrakis(triphenylphosphine)palladium
2: 88 percent / m-CPBA, Na2CO3
3: 95 percent / H2O / Li2CuCl4 (4 molpercent)
4: 78 percent / H2, p-toluene sulfonic acid / palladium black / ethanol
View Scheme
105873-61-8

4-Isopropenyl-2-phenyl-[1,3]dioxolane

74563-64-7

3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 88 percent / m-CPBA, Na2CO3
2: 95 percent / H2O / Li2CuCl4 (4 molpercent)
3: 78 percent / H2, p-toluene sulfonic acid / palladium black / ethanol
View Scheme
105873-62-9

4-(1,2-epoxy-1-methylethyl)-2-phenyl-1,3-dioxolane

74563-64-7

3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 95 percent / H2O / Li2CuCl4 (4 molpercent)
2: 78 percent / H2, p-toluene sulfonic acid / palladium black / ethanol
View Scheme
74563-64-7

3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane

75-36-5

acetyl chloride

C22H44O4

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at -70 - 20℃; for 4h;34%
74563-64-7

3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane

98-59-9

p-toluenesulfonyl chloride

519753-34-5

C27H48O5S

Conditions
ConditionsYield
Stage #1: 3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane; p-toluenesulfonyl chloride In hexane at 20℃; for 0.166667h;
Stage #2: With triethylamine; pyridine In hexane at 0 - 20℃; for 12h;
74563-64-7

3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane

67-64-1

acetone

518991-65-6

C23H46O3

Conditions
ConditionsYield
toluene-4-sulfonic acid for 15h; Heating / reflux;
74563-64-7

3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane

C40H81NO4

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: triethylamine / chloroform / 12 h / 0 - 20 °C
2: triethylamine / chloroform / 10 h / Reflux
3: triethylamine / chloroform / 5 h / 0 - 20 °C
View Scheme
74563-64-7

3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane

C22H47NO3

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / chloroform / 12 h / 0 - 20 °C
2: triethylamine / chloroform / 10 h / Reflux
View Scheme
74563-64-7

3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane

98-59-9

p-toluenesulfonyl chloride

C27H48O4S

Conditions
ConditionsYield
With triethylamine In chloroform at 0 - 20℃; for 12h;
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     China (Mainland)  |  Contact Details

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    Nanjing Raymon Biotech Co., Ltd. is specialized in developing and marketing middle & high level pharmaceutical intermediates. We are supplying different categories of high-quality

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