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CAS No.: | 74563-64-7 | ||||
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Name: | PHYTANTRIOL | ||||
Article Data: | 3 | ||||
Molecular Structure: | |||||
Formula: | C20H42 O3 | ||||
Molecular Weight: | 330.552 | ||||
Synonyms: | Phytanetriol;Phytantriol | ||||
Density: | 0.932 g/mL at 25oC(lit.) | ||||
Melting Point: | 56-57° | ||||
Boiling Point: | 130oC0.01 mm Hg(lit.) | ||||
Flash Point: | 199oC | ||||
Solubility: | 352μg/L at 20℃ | ||||
Safety: |
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PSA: | 60.69000 | ||||
LogP: | 4.52970 |
6,10,14-Trimethyl-2-(2-phenyl-[1,3]dioxolan-4-yl)-pentadecan-2-ol
3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane
Conditions | Yield |
---|---|
With hydrogen; toluene-4-sulfonic acid; palladium In ethanol | 78% |
2-methyl-3,4-epoxy-1-butene
3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 72 percent / tetrakis(triphenylphosphine)palladium 2: 88 percent / m-CPBA, Na2CO3 3: 95 percent / H2O / Li2CuCl4 (4 molpercent) 4: 78 percent / H2, p-toluene sulfonic acid / palladium black / ethanol View Scheme |
4-Isopropenyl-2-phenyl-[1,3]dioxolane
3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 88 percent / m-CPBA, Na2CO3 2: 95 percent / H2O / Li2CuCl4 (4 molpercent) 3: 78 percent / H2, p-toluene sulfonic acid / palladium black / ethanol View Scheme |
4-(1,2-epoxy-1-methylethyl)-2-phenyl-1,3-dioxolane
3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 95 percent / H2O / Li2CuCl4 (4 molpercent) 2: 78 percent / H2, p-toluene sulfonic acid / palladium black / ethanol View Scheme |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at -70 - 20℃; for 4h; | 34% |
3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane
p-toluenesulfonyl chloride
C27H48O5S
Conditions | Yield |
---|---|
Stage #1: 3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane; p-toluenesulfonyl chloride In hexane at 20℃; for 0.166667h; Stage #2: With triethylamine; pyridine In hexane at 0 - 20℃; for 12h; |
Conditions | Yield |
---|---|
toluene-4-sulfonic acid for 15h; Heating / reflux; |
3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: triethylamine / chloroform / 12 h / 0 - 20 °C 2: triethylamine / chloroform / 10 h / Reflux 3: triethylamine / chloroform / 5 h / 0 - 20 °C View Scheme |
3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / chloroform / 12 h / 0 - 20 °C 2: triethylamine / chloroform / 10 h / Reflux View Scheme |
3,7,11,15-tetramethyl-1,2,3-trihydroxyhexadecane
p-toluenesulfonyl chloride
Conditions | Yield |
---|---|
With triethylamine In chloroform at 0 - 20℃; for 12h; |