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| CAS No.: | 55896-93-0 |
|---|---|
| Name: | ACETIC ACID |
| Article Data: | 20 |
| Molecular Structure: | |
|
|
|
| Formula: | C4H7ClO4S |
| Molecular Weight: | 186.616 |
| Synonyms: | Acetic acid,(chlorosulfonyl)-, ethyl ester (9CI);(Chlorosulfonyl)acetic acid ethyl ester;2-(Chlorosulfonyl)acetic acid ethyl ester;Ethoxycarbonylmethanesulfonylchloride;Ethyl 2-(chlorosulfonyl)acetate;Ethyl2-(chlorosulfonyl)ethanoate; |
| EINECS: | 200-580-7 |
| Density: | 1.43 g/cm3 |
| Melting Point: | 16.2 °C(lit.) |
| Boiling Point: | 244.28 °C at 760 mmHg |
| Flash Point: | 101.537 °C |
| Hazard Symbols: |
 C
|
| Risk Codes: | 34 |
| Safety: | 23-26-45 |
| Transport Information: | UN 2790 8/PG 2 |
| PSA: | 68.82000 |
| LogP: | 1.19890 |
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sodium 2-ethoxy-2-oxoethane-1-sulfonate
- 55896-93-0
ethyl 2-(chlorosulfonyl)acetate
| Conditions | Yield |
|---|---|
| With trichlorophosphate at 80℃; for 2h; | 92% |
| With phosphorus pentachloride at 100℃; for 0.75h; Inert atmosphere; | 85% |
| With phosphorus pentachloride at 20℃; for 0.333333h; | 65% |
- 89124-45-8
acetic acid ethylester sulfonic acid
- 55896-93-0
ethyl 2-(chlorosulfonyl)acetate
| Conditions | Yield |
|---|---|
| With trichlorophosphate | 80% |
| With thionyl chloride at 120℃; | |
| With trichlorophosphate at 125℃; | |
| With trichlorophosphate | |
| With trichlorophosphate |
- 623-51-8
ethyl 2-sulfanylacetate
- 55896-93-0
ethyl 2-(chlorosulfonyl)acetate
| Conditions | Yield |
|---|---|
| With water; chlorine In dichloromethane at 30℃; for 1h; Cooling with acetone-dry ice; | 70% |
- 105-39-5
chloroacetic acid ethyl ester
- 55896-93-0
ethyl 2-(chlorosulfonyl)acetate
| Conditions | Yield |
|---|---|
| Stage #1: chloroacetic acid ethyl ester With sodium sulfite In ethanol; water for 6h; Heating; Stage #2: With oxalyl dichloride In N,N-dimethyl-formamide; toluene at 100℃; for 3h; Further stages.; | 59% |
| Conditions | Yield |
|---|---|
| In diethyl ether at 0℃; for 3h; Inert atmosphere; | 55% |
| at -12℃; | |
| In benzene for 1h; Heating; |
- 55896-93-0
ethyl 2-(chlorosulfonyl)acetate
- 470477-78-2
ethyl N-[4-(1-methylpiperidin-4-yloxy)-3-trifluoromethylphenyl]sulfamoylacetate
| Conditions | Yield |
|---|---|
| With pyridine In dichloromethane at 0 - 20℃; for 1h; | 100% |
- 55896-93-0
ethyl 2-(chlorosulfonyl)acetate
| Conditions | Yield |
|---|---|
| With 1H-imidazole In tetrahydrofuran at 20℃; Inert atmosphere; | 100% |
- 55896-93-0
ethyl 2-(chlorosulfonyl)acetate
- 877-80-5
N-methyl-4-nitrobenzylideneamine
| Conditions | Yield |
|---|---|
| With pyridine In tetrahydrofuran at 20℃; for 24h; Reagent/catalyst; Staudinger Ketene Cycloaddition; diastereoselective reaction; | 99% |
- 55896-93-0
ethyl 2-(chlorosulfonyl)acetate
- 96649-05-7
3-(methoxymethoxy)aniline
- 1049708-54-4
{N-[3-(methoxymethoxy)phenyl]sulfamoyl}acetate
| Conditions | Yield |
|---|---|
| With pyridine In dichloromethane at 0℃; for 2.5h; | 97% |
| Conditions | Yield |
|---|---|
| With 1H-imidazole In tetrahydrofuran | 96% |
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Chemistry
Product Name: Ethyl (chlorosulfonyl)acetate (CAS NO.55896-93-0)
Molecular Formula: C4H7ClO4S
Molecular Weight: 186.614g/mol
Mol File: 55896-93-0.mol
Boiling point: 244.28 °C at 760 mmHg
Flash Point: 101.537 °C
Density: 1.43 g/cm3
Surface Tension: 44.87 dyne/cm
Enthalpy of Vaporization: 48.133 kJ/mol
Vapour Pressure: 0.031 mmHg at 25°C