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CAS No.: | 4405-13-4 |
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Name: | GLYOXAL HYDRATE TRIMER |
Molecular Structure: | |
Formula: | C6H10O8 |
Molecular Weight: | 210.141 |
Synonyms: | GLYOXAL HYDRATE (TRIMER) FOR SYNTHESIS;glyoxal trimeric dihydrate;trimeric glyoxal dihydrate;glyoxal trimertetrahydrate;triglyoxal dihydrate;Triethanedialdihydrate;glyoxal trimer dihydrate;Glyoxal trimer dihydrate,Ethanedial;hexahydro[1,4]dioxino[2,3-b][1,4]dioxine-2,3,6,7-tetrol;Ethanedial,trimer,dihydrate;GLYOXAL TRIMER;Glyoxal Dihydrate; |
Density: | 1.9g/cm3 |
Melting Point: | 179 - 182°C |
Boiling Point: | 453.2°Cat760mmHg |
Flash Point: | 227.9°C |
Hazard Symbols: | Xi |
Risk Codes: | R36/37/38 |
PSA: | 117.84000 |
LogP: | -2.99420 |
(S)-1-phenyl-ethylamine
glyoxal trimer dihydrate
N,N'-bis<(S)-1-phenylethyl>ethanediimine
Conditions | Yield |
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With magnesium sulfate In dichloromethane for 5h; | 100% |
glyoxal trimer dihydrate
1,4,7,10-tetraazacyclododecan
cyclen-glyoxal
Conditions | Yield |
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In methanol at 0℃; for 3h; | 99% |
In methanol at 0 - 20℃; for 2.5h; | 94% |
In methanol; water at 20℃; for 3h; | 82% |
(S)-1-(4-methoxyphenyl)ethylamine
glyoxal trimer dihydrate
Conditions | Yield |
---|---|
In ethanol for 0.333333h; Reflux; | 96% |
Conditions | Yield |
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In isopropyl alcohol for 1h; Reflux; | 96% |
Conditions | Yield |
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In isopropyl alcohol for 1h; Reflux; | 95% |
Conditions | Yield |
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Stage #1: glyoxal trimer dihydrate With ammonium acetate; ammonia In tetrahydrofuran at -78℃; for 0.833333h; Inert atmosphere; Stage #2: cyclohexanone In tetrahydrofuran at -78 - 23℃; for 8h; Inert atmosphere; | 90% |
Conditions | Yield |
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With isopropyl alcohol at 50 - 55℃; for 1h; | 90% |
1,4,8,11-Tetraazacyclotetradecane
glyoxal trimer dihydrate
decahydro-1H,6H-3a,5a,8a,10a-tetraazapyrene
Conditions | Yield |
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In methanol; water at 20℃; for 2h; | 87% |
N,N'-dimethylsulfamide
glyoxal trimer dihydrate
Conditions | Yield |
---|---|
With hydrogenchloride at 35 - 40℃; for 1.5h; | 85% |
(S)-tert-butyl 7-(((benzyloxy)carbonyl)amino)-8-oxooctanoate
glyoxal trimer dihydrate
(5)-tert-butyl 7-(((benzyloxy)carbonyl)amino)-7-(1H-imidazol-2-yl)heptanoate
Conditions | Yield |
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With ammonia In methanol at 20℃; for 72h; Sealed tube; | 85% |
With ammonia In methanol at 20℃; for 72h; Sealed tube; |