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CAS No.: | 33528-63-1 |
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Name: | 1,12-DIMERCAPTODODECANE |
Article Data: | 6 |
Molecular Structure: | |
Formula: | C12H26 S2 |
Molecular Weight: | 234.47 |
Synonyms: | 1,12-DODECANEDITHIOL;1,12-DIMERCAPTODODECANE |
Density: | 0.92g/cm3 |
Boiling Point: | 329.7°C at 760 mmHg |
Flash Point: | 131.1°C |
PSA: | 77.60000 |
LogP: | 4.74700 |
thioacetic acid S-(12-acetylsulfanyldodecyl) ester
dodecane-1,12-dithiol
Conditions | Yield |
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With sodium hydroxide In water; acetone at 20℃; for 4h; | 56% |
1,12-dibromododecane
dodecane-1,12-dithiol
Conditions | Yield |
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With methanol; ammonium sulfide | |
With sodium hydrogensulfide; diethyl ether; ethanol; hydrogen sulfide zuletzt unter Erwaermen; | |
Multi-step reaction with 2 steps 1: 21 percent / dimethylformamide / 24 h / 20 °C 2: 56 percent / NaOH / H2O; acetone / 4 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: H2O / 20 h / Heating 2: 0.42 mmol / aq. NaOH / 6 h / Heating View Scheme |
diethyl ether
ethanol
1,12-dibromododecane
hydrogen sulfide
dodecane-1,12-dithiol
dodecane-1,12-dithiol
Conditions | Yield |
---|---|
With sodium hydroxide for 6h; Heating; | 0.42 mmol |
1,12-bis-carbamimidoylmercapto-dodecane
dodecane-1,12-dithiol
Conditions | Yield |
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With sodium hydroxide Heating; |
1,12-dodecandiol
dodecane-1,12-dithiol
Conditions | Yield |
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Multi-step reaction with 2 steps 1: aq. HBr / Heating 2: aq. NaOH / Heating View Scheme |
dodecane-1,12-dithiol
16,20-bis(bromomethyl)[14]paracyclophane
2,15-dithia[16][14]metaparacyclophane
Conditions | Yield |
---|---|
With caesium carbonate In ethanol; benzene for 6h; | 82% |
dodecane-1,12-dithiol
trityl chloride
1,12-Bis(triphenylmethylthio)dodecan
Conditions | Yield |
---|---|
With aluminum oxide In 1,4-dioxane for 24h; | 81% |
2-chloromethyl-3-chloroprop-1-ene
dodecane-1,12-dithiol
3-Methylene-1,5-dithia-cycloheptadecane
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 55 - 60℃; | 75% |
dodecane-1,12-dithiol
1,2-Bis<3-(bromomethyl)phenyl>-4,4-dimethyl-3,5-pyrazolidinedione
23,24-(Dimethylmalonyl)-2,15-dithia-23,24-diaza<16.2>metacyclophan
Conditions | Yield |
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With 18-crown-6 ether; potassium carbonate In tetrahydrofuran for 50h; Heating; | 64% |