N,N-DIMETHYLACETAMIDE-D9

Base Information

• Chemical Name: N,N-DIMETHYLACETAMIDE-D9
• CAS No.: 16727-10-9
• Molecular Formula: C₄H₉NO
• Molecular Weight: 96.0501
• Hs Code.: 2845 90 10
• Mol file: 16727-10-9.mol

Synonyms:N,N-DIMETHYLACETAMIDE-D9;forNMRspectroscopy,deuterationdegree

Chemical Property of N,N-DIMETHYLACETAMIDE-D9

Chemical Property:

• Vapor Pressure: 1.76 hPa (20 °C)
• Melting Point: -20°C (lit.)
• Refractive Index: n20/D 1.438(lit.)
• Boiling Point: 165-166°C (1013 hPa)
• Flash Point: 70°C
• PSA: 20.31000
• Density: 1.033 g/mL at 25 °C
• LogP: 0.09450
• Storage Temp.: Store below +30°C.

Purity/Quality:

97% ^*data from raw suppliers

N,N-Dimethylacetamide-d9 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: N,N-Dimethylacetamide (D9, 99%) was useful in the manufacturing of hollow fiber solid oxide fuel cell with petal-like cross section.

Technology Process of N,N-DIMETHYLACETAMIDE-D9

There total 4 articles about N,N-DIMETHYLACETAMIDE-D9 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C2H(2)H6N*C3H(2)H6NO2 + tetradeuterioacetic acid (1186-52-3) → Perdeutero-N,N-dimethyl-acetamid (16727-10-9)

Guidance literature:

With aluminum oxide; at 250 ℃; for 1h;

DOI:10.1002/jlcr.1467

Reference yield:

paraformaldehyde-d2 (1664-98-8,43094-80-0) + 2,2,2-trideuterioacetamide (23724-60-9) → Perdeutero-N,N-dimethyl-acetamid (16727-10-9)

Guidance literature:

With dideuterioformic acid; for 24h; Heating;

DOI:10.1002/jlcr.1467

Reference yield:

iodomethane-d3 (865-50-9) + 2,2,2-trideuterioacetamide (23724-60-9) → Perdeutero-N,N-dimethyl-acetamid (16727-10-9)

Guidance literature:

DOI:10.1002/jlcr.1467

upstream raw materials:

tetradeuterioacetic acid

paraformaldehyde-d2

2,2,2-trideuterioacetamide

iodomethane-d3

Refernces