(²H₃)-methyl nitrite

Base Information

• Chemical Name: (²H₃)-methyl nitrite
• CAS No.: 63562-23-2
• Molecular Formula: CH₃NO₂
• Molecular Weight: 64.0165
• Mol file: 63562-23-2.mol

Synonyms:(²H₃)-methyl nitrite

Chemical Property of (²H₃)-methyl nitrite

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (²H₃)-methyl nitrite

There total 1 articles about (²H₃)-methyl nitrite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,1-trideuteromethanol (1849-29-2) → paraformaldehyde-d2 (1664-98-8,43094-80-0) + methane-d3 (676-80-2) + nitromethane-d3 (13031-32-8) + dideuterio-hydroxy-methyl (79825-55-1) + (2H3)-methyl nitrite (63562-23-2) + carbon dioxide (124-38-9,18923-20-1) + D2-nitrosomethanol

Guidance literature:

With nitrogen(II) oxide; Radiolysis;

DOI:10.1021/acs.jpca.7b12235

Reference yield:

(2H3)-methyl nitrite (63562-23-2) + fluorine → nitrogen hypofluoride (11094-71-6) + nitrogen(II) oxide (10102-43-9) + nitrosyl fluoride (7789-25-5)

Guidance literature:

byproducts: CD3O, D2CO, DF; Irradiation (UV/VIS); Hg-arc irradiation; not separated, detected by IR;

DOI:10.1021/j150642a035

Reference yield:

(2H3)-methyl nitrite (63562-23-2) → paraformaldehyde-d2 (1664-98-8,43094-80-0)

Guidance literature:

In solid; at -259.2 ℃; for 4.85h; Irradiation;

DOI:10.1021/j100212a019

upstream raw materials:

1,1,1-trideuteromethanol

Downstream raw materials:

paraformaldehyde-d2

nitrogen hypofluoride

nitrogen(II) oxide

nitrosyl fluoride

Refernces