Technology Process of Phosphonic acid, (4-amino-1-hydroxybutylidene)bis-, monosodium salt
There total 7 articles about Phosphonic acid, (4-amino-1-hydroxybutylidene)bis-, monosodium salt which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4-amino-n-butyric acid;
With
phosphonic Acid; methanesulfonic acid; phosphorus trichloride;
at 65 ℃;
With
water;
Reflux;
With
sodium hydroxide;
In
water;
DOI:10.1021/bc400317h
- Guidance literature:
-
tetraethyl 2-N-phthalimide-1-hydroxybutylidene-1,1-bisphosphonate;
With
hydrogenchloride;
Heating;
With
sodium hydroxide;
pH=4.3 - 4.4;
DOI:10.1080/10426500108045257
- Guidance literature:
-
In
water; butanone;
at 2.3 - 72 ℃;
for 1.16667 - 2h;
Purification / work up;