144708-85-0Relevant articles and documents
New efficient method of alkoxymethyl etherification of secondary alcohols
Watanabe, Yosuke,Ikemoto, Tetsuya
, p. 5795 - 5797 (2004)
A new efficient method of MOM etherification of secondary alcohols using 2-(chloromethyl)-3,5-dioxahex-1-ene (Okahara's reagent) is reported.
Method for preparing tertiary alkyl trifluoromethyl sulfide
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Paragraph 0027-0030, (2018/10/19)
The invention discloses a method for preparing tertiary alkyl trifluoromethyl sulfide. The method includes: using tertiary alkoxy ether as a raw material; under illumination of blue light, in a solution, in an argon atmosphere and at the presence of a small amount of potassium carbonate, reacting with 2-((trifluoromethyl)thio) isoindoline-1, 3-diketone at room temperature through synergistic catalysis of a photocatalyst 4CzIPN and an organic thiol catalyst 4-thionaphthol[2, 1-d:1', 2'-f][1, 3, 2]dioxocycloheptene-4-oxide, wherein the photocatalyst 4CzIPN and the organic thiol catalyst have following structures.
HYDROXY-PROTECTING REAGENT AND METHOD OF PROTECTING HYDROXY WITH THE SAME
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Page/Page column 10-11, (2008/06/13)
The present invention relates to a method of protecting a hydroxyl group, which includes reacting a hydroxyl group-containing compound with a compound represented by the formula (I) : wherein R is a phenyl group optionally having substituent(s), an alkyl