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  • 13752-51-7 Structure
  • Basic information

    1. Product Name: 4-[(4-Morpholinylthio)thioxomethyl]-morpholine
    2. Synonyms: 4-[(4-Morpholinylthio)thioxomethyl]-morpholine;ACCELERATOR OTOS;CURE-RITE 18;N-OXYDIETHYLENE THIOCARBAMYL-N-OXYDIETHYLENE SULFENAMIDE;morpholin-4-yl morpholine-4-carbodithioate;4-((4-morpholinylthio)thioxomethyl)-morpholin;4-((morpholinothiocarbonyl)thio)-morpholin;4-((morpholinothiocarbonyl)thio)morpholine
    3. CAS NO:13752-51-7
    4. Molecular Formula: C9H16N2O2S2
    5. Molecular Weight: 248.37
    6. EINECS: 237-335-9
    7. Product Categories: N/A
    8. Mol File: 13752-51-7.mol
    9. Article Data: 2
  • Chemical Properties

    1. Melting Point: 139 °C
    2. Boiling Point: 378.1 °C at 760 mmHg
    3. Flash Point: 182.4 °C
    4. Appearance: /
    5. Density: 1.2971 (rough estimate)
    6. Vapor Pressure: 6.45E-06mmHg at 25°C
    7. Refractive Index: 1.6800 (estimate)
    8. Storage Temp.: N/A
    9. Solubility: N/A
    10. PKA: 1.08±0.20(Predicted)
    11. Water Solubility: 127mg/L at 20℃
    12. CAS DataBase Reference: 4-[(4-Morpholinylthio)thioxomethyl]-morpholine(CAS DataBase Reference)
    13. NIST Chemistry Reference: 4-[(4-Morpholinylthio)thioxomethyl]-morpholine(13752-51-7)
    14. EPA Substance Registry System: 4-[(4-Morpholinylthio)thioxomethyl]-morpholine(13752-51-7)
  • Safety Data

    1. Hazard Codes: N/A
    2. Statements: N/A
    3. Safety Statements: N/A
    4. WGK Germany:
    5. RTECS:
    6. HazardClass: N/A
    7. PackingGroup: N/A
    8. Hazardous Substances Data: 13752-51-7(Hazardous Substances Data)

13752-51-7 Usage

Uses

Acceleratorotos is an accelerator; used in preparation of a Rubber anti-fatigue agent.

Safety Profile

Experimental reproductive effects. Mutation data reported. When heated to decomposition it emits toxic vapors of NOx and SOx.

Check Digit Verification of cas no

The CAS Registry Mumber 13752-51-7 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 1,3,7,5 and 2 respectively; the second part has 2 digits, 5 and 1 respectively.
Calculate Digit Verification of CAS Registry Number 13752-51:
(7*1)+(6*3)+(5*7)+(4*5)+(3*2)+(2*5)+(1*1)=97
97 % 10 = 7
So 13752-51-7 is a valid CAS Registry Number.
InChI:InChI=1/C9H16N2O2S2/c14-9(10-1-5-12-6-2-10)15-11-3-7-13-8-4-11/h1-8H2

13752-51-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 17, 2017

Revision Date: Aug 17, 2017

1.Identification

1.1 GHS Product identifier

Product name morpholin-4-yl morpholine-4-carbodithioate

1.2 Other means of identification

Product number -
Other names Morpholino-thiocarbamoyl-sulfensaeuremorpholid

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Process regulators
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:13752-51-7 SDS

13752-51-7Synthetic route

morpholine
110-91-8

morpholine

acetyl-trichloromethyl-disulfane
72087-88-8

acetyl-trichloromethyl-disulfane

4-(morpholine-4-carbothioylsulfanyl)-morpholine
13752-51-7

4-(morpholine-4-carbothioylsulfanyl)-morpholine

Conditions
ConditionsYield
In diethyl ether Mechanism; further α-chloroalkyd disulfides, <18 deg C;32%
In diethyl ether <18 deg C;22%

13752-51-7Downstream Products

13752-51-7Relevant articles and documents

STUDIES OF DITHIIRANES AND THIOSULFINES AS REACTIVE INTERMEDIATES

Senning, Alexander,Hansen, Holger C.,Abdel-Megeed, Mohamed F.,Mazurkiewicz, Witold,Jensen, Birgit

, p. 739 - 746 (2007/10/02)

Indirect, but compelling evidence for the intermediacy of dithiiranes 1 and thiosulfines 2 has been found by us and is also provided by literature data.The intriguing dithiirane -> dithioester rearrangement as well as most of the interrelations and conversions postulated in Scheme 1 have been demonstrated experimentally.In a number of cases acetyl α-chloroalkyl disulfides 16 (X=Cl, Y=COCH3) are useful starting materials for the synthesis of thioamides such as 40.

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