Technology Process of 1-(2-bromo-5-methyl-naphthalen-1-yloxy)-propan-2-one
There total 5 articles about 1-(2-bromo-5-methyl-naphthalen-1-yloxy)-propan-2-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
Heating;
DOI:10.1039/b001859g
- Guidance literature:
-
Multi-step reaction with 5 steps
1: diethyl ether / 1 h / Heating
2: 10percent Pd/C / triethylene glycol dimethyl ether / 48 h / Heating
3: BBr3 / CH2Cl2 / -78 - 20 °C
4: 70 percent / NBS / CH2Cl2 / 0 °C
5: 96 percent / K2CO3 / acetone / Heating
With
N-Bromosuccinimide; boron tribromide; potassium carbonate;
10percent Pd/C;
In
diethyl ether; Triethylene glycol dimethyl ether; dichloromethane; acetone;
1: Grignard reaction / 2: Aromatization / 3: Demethylation / 4: Bromination / 5: Alkylation;
DOI:10.1039/b001859g
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 10percent Pd/C / triethylene glycol dimethyl ether / 48 h / Heating
2: BBr3 / CH2Cl2 / -78 - 20 °C
3: 70 percent / NBS / CH2Cl2 / 0 °C
4: 96 percent / K2CO3 / acetone / Heating
With
N-Bromosuccinimide; boron tribromide; potassium carbonate;
10percent Pd/C;
In
Triethylene glycol dimethyl ether; dichloromethane; acetone;
1: Aromatization / 2: Demethylation / 3: Bromination / 4: Alkylation;
DOI:10.1039/b001859g