C₂₄H₃₄N₂O₄

Base Information

• Chemical Name: C₂₄H₃₄N₂O₄
• CAS No.: 1362626-92-3
• Molecular Formula: C₂₄H₃₄N₂O₄
• Molecular Weight: 414.545
• Mol file: 1362626-92-3.mol

Synonyms:

Chemical Property of C₂₄H₃₄N₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₃₄N₂O₄

There total 6 articles about C₂₄H₃₄N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isovanillin (621-59-0) → C24H34N2O4 (1362626-92-3)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 12 h / Inert atmosphere; Reflux

2: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / water; acetonitrile / 0 - 10 °C

3: diphenyl phosphoryl azide; triethylamine / benzene / 5 h / 20 °C / Inert atmosphere; Reflux

4: dichloromethane / 0.17 h / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; diphenyl phosphoryl azide; dihydrogen peroxide; potassium carbonate; triethylamine; In dichloromethane; water; acetone; acetonitrile; benzene; 3: Curtius rearrangement;

DOI:10.1021/ml300005w

Reference yield:

3-(4-methyl-pentyloxy)-4-methoxy-benzaldehyde → C24H34N2O4 (1362626-92-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / water; acetonitrile / 0 - 10 °C

2: diphenyl phosphoryl azide; triethylamine / benzene / 5 h / 20 °C / Inert atmosphere; Reflux

3: dichloromethane / 0.17 h / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; diphenyl phosphoryl azide; dihydrogen peroxide; triethylamine; In dichloromethane; water; acetonitrile; benzene; 2: Curtius rearrangement;

DOI:10.1021/ml300005w

Reference yield:

3-(4-methyl-pentyloxy)-4-methoxy-benzoic acid → C24H34N2O4 (1362626-92-3)

Guidance literature:

Multi-step reaction with 2 steps

1: diphenyl phosphoryl azide; triethylamine / benzene / 5 h / 20 °C / Inert atmosphere; Reflux

2: dichloromethane / 0.17 h / Inert atmosphere

With diphenyl phosphoryl azide; triethylamine; In dichloromethane; benzene; 1: Curtius rearrangement;

DOI:10.1021/ml300005w

upstream raw materials:

isovanillin

(S)-(-)-N-(2-hydroxyethyl)-α-methylbenzylamine

1-bromo-5-methylpentane

Refernces

• 1、 Zhang, Mei,Yang, Xiao-Ying,Tang, Wei,Groeneveld, Tom W. L.,He, Pei-Lan,Zhu, Feng-Hua,Li, Jia,Lu, Wei,Blom, Anna M.,Zuo, Jian-Ping,Nan, Fa-Jun. "Discovery and structural modification of 1-phenyl-3-(1-phenylethyl)urea derivatives as inhibitors of complement". . p. 317 - 321. Retrieved 2012/05/20.