3-BENZYLOXY-2-METHYL-1-PROPANOL

Base Information

• Chemical Name: 3-BENZYLOXY-2-METHYL-1-PROPANOL
• CAS No.: 56850-59-0
• Molecular Formula: C₁₁H₁₆O₂
• Molecular Weight: 180.247
• Hs Code.: 2909499000
• Mol file: 56850-59-0.mol

Synonyms:3-(Benzyloxy)-2-methyl-1-propanol;

Chemical Property of 3-BENZYLOXY-2-METHYL-1-PROPANOL

Chemical Property:

• Vapor Pressure: 0.000565mmHg at 25°C
• Refractive Index: 1.513
• Boiling Point: 298.5 °C at 760 mmHg
• Flash Point: 126.5 °C
• PSA: 29.46000
• Density: 1.023 g/cm³
• LogP: 1.83160

Purity/Quality:

99% ^*data from raw suppliers

3-BENZYLOXY-2-METHYL-1-PROPANOL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-BENZYLOXY-2-METHYL-1-PROPANOL

There total 18 articles about 3-BENZYLOXY-2-METHYL-1-PROPANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

5-methyl-2-phenyl-[1,3]dioxane (27942-89-8) → 3-(benzyloxy)-2-methylpropan-1-ol (63930-46-1,63930-49-4,56850-59-0,64839-09-4)

Guidance literature:

With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether;

DOI:10.1016/S0040-4039(99)01951-6

Reference yield: 91.0%

4-(3-Benzyloxy-2-methyl-propoxymethyl)-1,5-dimethoxy-naphthalene (126309-00-0) → 3-(benzyloxy)-2-methylpropan-1-ol (63930-46-1,63930-49-4,56850-59-0,64839-09-4)

Guidance literature:

With terephthalonitrile; magnesium(II) perchlorate; In acetonitrile; for 1.5h; Ambient temperature; Irradiation;

Reference yield: 90.5%

→ 3-(benzyloxy)-2-methylpropan-1-ol (63930-46-1,63930-49-4,56850-59-0,64839-09-4)

Guidance literature:

upstream raw materials:

((2-methylallyloxy)methyl)benzene

Benzyl 3-(phenylmethoxy)-2-methylpropanoate

2-methyl-1.3-propanediol

benzyl bromide

Downstream raw materials:

3-benzyloxy-2-methyl-1-propyl bromide

4-benzyloxy-3-methylbut-1-yne

2-(1-(benzyloxy)propan-2-yl)-5-mesityl-6-oxo-3,6-dihydro-2H-pyran-4-yl pivalate

6-(1-(benzyloxy)propan-2-yl)-3-mesityldihydro-2H-pyran-2,4-(3H)-dione

Refernces

• 1、 -. "SUBSTITUTED HETEROARYL COMPOUNDS AND METHODS OF USE". Paragraph 0468. . Retrieved 2017/04/14.
• 2、 -. "DIHYDROPYRONE COMPOUNDS AND HERBICIDES COMPRISING THE SAME". Paragraph 0088. . Retrieved 2014/06/23.