diethyl S-(phenylthio)methyl phosphorodithioate

Base Information

• Chemical Name: diethyl S-(phenylthio)methyl phosphorodithioate
• CAS No.: 25795-00-0
• Molecular Formula: C₁₁H₁₇O₂PS₃
• Molecular Weight: 308.427
• Mol file: 25795-00-0.mol

Synonyms:

Chemical Property of diethyl S-(phenylthio)methyl phosphorodithioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diethyl S-(phenylthio)methyl phosphorodithioate

There total 7 articles about diethyl S-(phenylthio)methyl phosphorodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

phenylthiomethyl chloride (7205-91-6) + potassium O,O-diethyldithiophosphate (3454-66-8) → diethyl S-(phenylthio)methyl phosphorodithioate (25795-00-0)

Guidance literature:

In dichloromethane; for 3h; Ambient temperature;

Reference yield:

thiophenol (108-98-5) → diethyl S-(phenylthio)methyl phosphorodithioate (25795-00-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 15.1 percent / 35percent hydrochloric acid / 1.5 h / 40 °C

2: 83 percent / CH₂Cl₂ / 3 h / Ambient temperature

With hydrogenchloride; In dichloromethane;

Reference yield:

benzenesulfenyl chloride (931-59-9) → diethyl S-(phenylthio)methyl phosphorodithioate (25795-00-0)

Guidance literature:

Multi-step reaction with 2 steps

2: diethyl ether / 3 h / Ambient temperature

In diethyl ether;

upstream raw materials:

phenylthiomethyl chloride

sodium O,O-diethyl phosphorodithioate

O,O-Diethyl hydrogen phosphorodithioate

diazomethane

Refernces