Ethanone, 1-(4-phenylcyclohexyl)-

Base Information

• Chemical Name: Ethanone, 1-(4-phenylcyclohexyl)-
• CAS No.: 23923-62-8
• Molecular Formula: C14H18O
• Molecular Weight: 202.296
• Mol file: 23923-62-8.mol

Synonyms:Ketone, methyl 4-phenylcyclohexyl (8CI);

Chemical Property of Ethanone, 1-(4-phenylcyclohexyl)-

Chemical Property:

• Vapor Pressure: 0.000481mmHg at 25°C
• Refractive Index: 1.519
• Boiling Point: 313.9 °C at 760 mmHg
• Flash Point: 132.1 °C
• PSA: 17.07000
• Density: 1.001 g/cm³
• LogP: 3.54940

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-(4-phenylcyclohexyl)-

There total 7 articles about Ethanone, 1-(4-phenylcyclohexyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

4-fenil-1-acetil-1-cicloesene (84871-22-7) → cis e trans-4-fenilacetilcicloesano (23923-62-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; Ambient temperature;

Reference yield: 70.0%

acetyl chloride (75-36-5) + cyclohexene (110-83-8) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → cis e trans-4-fenilacetilcicloesano (23923-62-8)

Guidance literature:

With aluminum (III) chloride; at 0 - 45 ℃; for 2h;

Reference yield:

acetyl chloride (75-36-5) + cyclohexene (110-83-8) → cis e trans-4-fenilacetilcicloesano (23923-62-8)

Guidance literature:

With carbon disulfide; aluminium trichloride; at -50 - -20 ℃; 1-<4-phenyl-cyclohexyl>-ethanon-(1) of mp: 55 degree Celsius; Erwaermen des vom Schwefelkohlenstoff befreiten Reaktionsgemisches mit Benzol auf 40-45grad;

DOI:10.1021/ja01223a001

upstream raw materials:

acetyl chloride

cyclohexene

benzene

4-fenil-1-acetil-1-cicloesene

Downstream raw materials:

(4-ethylcyclohexyl)benzene

trans-4-phenylcyclohexanecarboxylic acid

trans-4-phenylcyclohexyl acetate

4-phenylcyclohexene

Refernces

• 1、 Karamysheva, L. A.,Torgova, S. I.,Agafonova, I. F.,Geivandov, R. Kh.,Bykova, V. V.,Burylin, P. A.. "LIQUID-CRYSTALLINE COMPOUNDS OF THE ALICYCLIC SERIES III. SYNTHESIS AND ISOMORPHISM OF ETHERS AND ESTERS CONTAINING THE PHENYLCYCLOHEXANE FRAGMENT". . p. 736 - 741. Retrieved 2007/10/02.