Technology Process of N-[2-((2-isopropylbenzoyl)oxy)propyl]-N,N-dimethylcyclohexanaminium iodide
There total 4 articles about N-[2-((2-isopropylbenzoyl)oxy)propyl]-N,N-dimethylcyclohexanaminium iodide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
1,2-dichloro-ethane;
at 20 ℃;
for 16h;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane; water / 16 h / 20 °C / Cooling with ice
2: toluene / 16 h / 0 °C / Reflux
3: 1,2-dichloro-ethane / 16 h / 20 °C / Sealed tube
With
sodium tris(acetoxy)borohydride; acetic acid;
In
water; 1,2-dichloro-ethane; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ethanol / 0.17 h / 0 - 10 °C
1.2: 0.25 h / 0 - 20 °C
2.1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane; water / 16 h / 20 °C / Cooling with ice
3.1: toluene / 16 h / 0 °C / Reflux
4.1: 1,2-dichloro-ethane / 16 h / 20 °C / Sealed tube
With
sodium tris(acetoxy)borohydride; acetic acid;
In
ethanol; water; 1,2-dichloro-ethane; toluene;
