2,3-secoreserpine

Base Information Edit

Chemical Name:2,3-secoreserpine
CAS No.:16625-53-9
Molecular Formula:C₃₃H₄₂N₂O₉
Molecular Weight:610.704
Hs Code.:
Mol file:16625-53-9.mol

Synonyms:2,3-secoreserpine

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Chemical Property of 2,3-secoreserpine Edit

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Technology Process of 2,3-secoreserpine

There total 28 articles about 2,3-secoreserpine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 68104-24-5
6-methoxy-tryptophyl bromide

: 70617-03-7,96687-91-1
(4aR^*,5S^*,6S^*,7S^*,8aR^*)-6-methoxy-5-(methoxycarbonyl)-7-((3,4,5-trimethoxybenzoyl)oxy)perhydroisoquinoline

: 16625-53-9,96687-92-2,110013-47-3
2,3-seco-2,3-dihydroreserpine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; for 60h; Ambient temperature;
DOI:10.1021/ja00299a050

Reference yield:

: 482-85-9
Isoreserpin

: 50-55-5
reserpine

: 16625-52-8
C₃₃H₄₂N₂O₉

: 16625-53-9
2,3-secoreserpine

Guidance literature:: With acetic acid; zinc; for 12h; Heating;
DOI:10.1021/jo00280a052

Reference yield:

: 96648-91-8
(4aR^*,5S^*,6S^*,7R^*)-2-benzyl-3,4,4a,5,6,7-hexahydro-5-((methoxymethoxy)methyl)-6,7-oxy-1(2H)-isoquinolone

: 16625-53-9,96687-92-2,110013-47-3
2,3-seco-2,3-dihydroreserpine

Guidance literature:: Multi-step reaction with 11 steps

1: 90 percent / lithium 2-ethylhexanoate / 1,2-dimethoxy-ethane / 16 h / Heating

2: 98 percent / Ag₂O, CaSO₄ / 96 h / Ambient temperature

3: acid / methanol

4: pyridinium dichromate / dimethylformamide

6: alane

7: methanol / acid

8: 40 percent / hydrogen

9: 91 percent / 4-(dimethylamino)pyridine / pyridine; CH₂Cl₂ / 24 h / Ambient temperature

10: 93 percent / hydrogen / 20 percent Pd(OH)2/C / acetic acid / 24 h / 760 Torr

11: 69 percent / N,N-diisopropylethylamine, NaI / dimethylsulfoxide / 72 h / Ambient temperature

With methanol; dmap; calcium sulfate; dipyridinium dichromate; hydrogen; aluminium hydride; lithium 2-ethylhexanoate; N-ethyl-N,N-diisopropylamine; sodium iodide; silver(l) oxide; palladium dihydroxide; In pyridine; methanol; 1,2-dimethoxyethane; dichloromethane; acetic acid; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja00254a036