Technology Process of C31H26O8S4
There total 9 articles about C31H26O8S4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium fluoride; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride;
In
methanol; toluene;
at 80 ℃;
for 0.166667h;
Inert atmosphere;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride / toluene; methanol / 0.75 h / 60 °C / Inert atmosphere
2: N-Bromosuccinimide; acetic acid / chloroform / 3 h / 20 °C
3: [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; potassium fluoride / toluene; methanol / 0.17 h / 80 °C / Inert atmosphere; Sealed tube
With
potassium fluoride; N-Bromosuccinimide; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; potassium carbonate; acetic acid;
In
methanol; chloroform; toluene;
1: |Suzuki Coupling / 3: |Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: acetyl chloride / 20 °C / Reflux
2: potassium carbonate; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride / toluene; methanol / 0.75 h / 60 °C / Inert atmosphere
3: N-Bromosuccinimide; acetic acid / chloroform / 3 h / 20 °C
4: [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; potassium fluoride / toluene; methanol / 0.17 h / 80 °C / Inert atmosphere; Sealed tube
With
potassium fluoride; N-Bromosuccinimide; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; potassium carbonate; acetic acid; acetyl chloride;
In
methanol; chloroform; toluene;
2: |Suzuki Coupling / 4: |Suzuki Coupling;