decyl trifluoroacetate

Base Information

• Chemical Name: decyl trifluoroacetate
• CAS No.: 333-88-0
• Molecular Formula: C₁₂H₂₁F₃O₂
• Molecular Weight: 254.293
• Mol file: 333-88-0.mol

Synonyms:decyl trifluoroacetate

Chemical Property of decyl trifluoroacetate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of decyl trifluoroacetate

There total 1 articles about decyl trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Decanol (112-30-1) + dimethyl sulfoxide (67-68-5,8070-53-9) + trifluoroacetic anhydride (407-25-0) → caprinaldehyde (112-31-2) + decyl trifluoroacetate (333-88-0) + 1-methylsulfanylmethoxy-decane (57738-68-8)

Guidance literature:

With triethylamine; In dichloromethane; at -20 ℃; Further Variations:; Temperatures; Product distribution;

DOI:10.1002/anie.200462466

Reference yield: 97.0%

decyl trifluoroacetate (333-88-0) → 1-Decanol (112-30-1)

Guidance literature:

With silica gel; triethylamine; In diethyl ether; Petroleum ether;

DOI:10.1080/00304949909458329

Reference yield:

decyl trifluoroacetate (333-88-0) → 1-bromo dodecane (112-29-8)

Guidance literature:

With lithium bromide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; for 3h; Yield given; Heating;

DOI:10.1055/s-1987-27988

upstream raw materials:

1-Decanol

dimethyl sulfoxide

trifluoroacetic anhydride

Downstream raw materials:

1-bromo dodecane

1-Decanol

Refernces

• 1、 Kawaguchi, Tatsuya,Miyata, Hiroyuki,Ataka, Kikuo,Mae, Kazuhiro,Yoshida, Jun-Ichi. "Room-temperature Swern oxidations by using a microscale flow system". . p. 2413 - 2416. Retrieved 2007/10/03.