Technology Process of Ethanone, 1-(3,6-dihydroxy-2-methylphenyl)- (9CI)
There total 3 articles about Ethanone, 1-(3,6-dihydroxy-2-methylphenyl)- (9CI) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) n-BuLi / 1) hexane, ether, -70 deg C, 1.5 h, 2) -70 deg C, 2.5 h
2: 94 percent / MnO2 / diethyl ether / 24 h / Heating
3: 74 percent / AlCl3 / chlorobenzene / 4 h / Heating
With
manganese(IV) oxide; n-butyllithium; aluminium trichloride;
In
diethyl ether; chlorobenzene;
DOI:10.1080/00397919608003486
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) NaNO2, H2SO4, 2) KBr, HBr, CuBr / 1) water, less than 10 deg C, 2) 90-100 deg C, 0.5 h
2: 1) n-BuLi / 1) hexane, ether, -70 deg C, 1.5 h, 2) -70 deg C, 2.5 h
3: 94 percent / MnO2 / diethyl ether / 24 h / Heating
4: 74 percent / AlCl3 / chlorobenzene / 4 h / Heating
With
manganese(IV) oxide; n-butyllithium; aluminium trichloride; sulfuric acid; hydrogen bromide; potassium bromide; copper(I) bromide; sodium nitrite;
In
diethyl ether; chlorobenzene;
DOI:10.1080/00397919608003486
