2-nitro(dichloroiodo)benzene

Base Information

• Chemical Name: 2-nitro(dichloroiodo)benzene
• CAS No.: 827-28-1
• Molecular Formula: C₆H₄Cl₂INO₂
• Molecular Weight: 319.914
• Mol file: 827-28-1.mol

Synonyms:2-nitro(dichloroiodo)benzene

Chemical Property of 2-nitro(dichloroiodo)benzene

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-nitro(dichloroiodo)benzene

There total 1 articles about 2-nitro(dichloroiodo)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

o-nitroiodobenzene (609-73-4) → 2-nitro(dichloroiodo)benzene (827-28-1)

Guidance literature:

With hydrogenchloride; nitric acid; In acetic anhydride; acetic acid; at 20 ℃; for 2h;

Reference yield: 85.0%

2-nitro(dichloroiodo)benzene (827-28-1) → o-nitro-iodosylbenzene (69180-53-6)

Guidance literature:

With potassium hydroxide; In methanol; water; at 0 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/adsc.201700934

Reference yield:

2-nitro(dichloroiodo)benzene (827-28-1) → o-nitroiodobenzene (609-73-4)

Guidance literature:

beim Umkrystallisieren;

upstream raw materials:

o-nitroiodobenzene

Downstream raw materials:

o-nitroiodobenzene

o-nitro-iodosylbenzene

2-nitroiodobenzene diacetate

Refernces

• 1、 Tale, Nilesh P.,Shelke, Amol V.,Karade, Nandkishor N.. "Ceric ammonium nitrate as the novel oxidizing agent for the facile synthesis of (dichloroiodo)arenes". experimental part. p. 2959 - 2965. Retrieved 2012/07/27.
• 2、 Baranowski,Plachta,Skulski,Klimaszewska. "Liquid-phase and biphasic chlorination of some iodoarenes to form (dichloroiodo)arenes with sodium peroxodisulfate as the oxidant". . p. 435 - 437. Retrieved 2007/10/03.