1-IODO-4-(TRANS-4-N-PROPYLCYCLOHEXYL)BENZENE

Base Information

• Chemical Name: 1-IODO-4-(TRANS-4-N-PROPYLCYCLOHEXYL)BENZENE
• CAS No.: 111158-11-3
• Molecular Formula: C₁₅H₂₁I
• Molecular Weight: 328.236
• Hs Code.: 2903999090
• Mol file: 111158-11-3.mol

Synonyms:Benzene,1-iodo-4-(4-propylcyclohexyl)-, trans-;4-(trans-4-Propylcyclohexyl)-1-iodobenzene;4-Iodo-1-(trans-4-propylcyclohexyl)benzene;1-(trans-4-Propylcyclohexyl)-4-iodobenzene;

Chemical Property of 1-IODO-4-(TRANS-4-N-PROPYLCYCLOHEXYL)BENZENE

Chemical Property:

• Refractive Index: 1.553
• Boiling Point: 348.501 °C at 760 mmHg
• Flash Point: 157.979 °C
• PSA: 0.00000
• Density: 1.33 g/cm³
• LogP: 5.36510
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

99% ^*data from raw suppliers

1-Iodo-4-(trans-4-N-propylcyclohexyl)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-IODO-4-(TRANS-4-N-PROPYLCYCLOHEXYL)BENZENE

There total 2 articles about 1-IODO-4-(TRANS-4-N-PROPYLCYCLOHEXYL)BENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

4-(4-propylcyclohexyl)-1-bromobenzene (86579-53-5,167858-55-1) → 1-iodo-4-(4-propyl-cyclohexyl)-benzene (860639-66-3,111158-11-3)

Guidance literature:

With n-butyllithium; iodine; In tetrahydrofuran; at -78 ℃; for 1h;

DOI:10.1021/ol047311p

Reference yield:

→ 1-iodo-4-(4-propyl-cyclohexyl)-benzene (860639-66-3,111158-11-3)

Guidance literature:

With sulfuric acid; iodine; acetic acid; In water;

upstream raw materials:

4-(4-propylcyclohexyl)-1-bromobenzene

Refernces

• 1、 Stara, Irena G.,Alexandrova, Zuzana,Teply, Filip,Sehnal, Petr,Stary, Ivo,Saman, David,Budesinsky, Milos,Cvacka, Josef. "Asymmetric synthesis of [7]helicene-like molecules". . p. 2547 - 2550. Retrieved 2007/10/03.