1,2-DIMETHOXYBENZENE-3,4,5,6-D4

Base Information

• Chemical Name: 1,2-DIMETHOXYBENZENE-3,4,5,6-D4
• CAS No.: 126840-15-1
• Molecular Formula: C8H6D4O2
• Molecular Weight: 142.19
• Mol file: 126840-15-1.mol

Synonyms:1,2-Dimethoxybenzene-3,4,5,6-d₄;

Chemical Property of 1,2-DIMETHOXYBENZENE-3,4,5,6-D4

Chemical Property:

• Boiling Point: 206.25 °C at 760 mmHg
• Flash Point: 87.222 °C
• PSA: 18.46000
• Density: 1.035 g/cm³
• LogP: 1.70380

Purity/Quality:

99% ^*data from raw suppliers

1,2-Dimethoxybenzene-3,4,5,6-d4 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 1,2-Dimethoxybenzene-3,4,5,6-d4 (CAS# 126840-15-1) is a useful isotopically labeled research compound.

Technology Process of 1,2-DIMETHOXYBENZENE-3,4,5,6-D4

There total 3 articles about 1,2-DIMETHOXYBENZENE-3,4,5,6-D4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-dimethoxybenzene (91-16-7) → [3,4,5,6-2H4]-1,2-dimethoxybenzene (126840-15-1)

Guidance literature:

With [D₃]phosphoric acid; In water-d2; at 80 ℃; for 48h; Yield given;

DOI:10.1021/ja00198a018

Reference yield:

4,5-Dichlor-brenzcatechindimethylether (2772-46-5) → [3,4,5,6-2H4]-1,2-dimethoxybenzene (126840-15-1) + C8H7(2)HCl2O2 + C8H6(2)H3ClO2 + C8H6(2)H2Cl2O2 (113440-41-8)

Guidance literature:

With tetrabutylammonium perchlorate; water-d2; In N,N-dimethyl-formamide; at 25 - 30 ℃; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1021/jo00299a037

Reference yield:

→ [3,4,5,6-2H4]-1,2-dimethoxybenzene (126840-15-1)

Guidance literature:

aus 4-Iod-veratrol 1. Butyl-Li, Ae.; 2. D2O;

upstream raw materials:

1,2-dimethoxybenzene

4,5-Dichlor-brenzcatechindimethylether

Refernces

• 1、 Kimura, Makoto,Miyahara, Hiroyoshi,Moritani, Noriyuki,Sawaki, Yasuhiko. "Electroreductive Dehalogenation of Chlorinated Aromatic Ethers. Unexpected Electrogenerated Base Catalyzed Reactions". . p. 3897 - 3902. Retrieved 2007/10/02.