Technology Process of C42H50O10S2
There total 3 articles about C42H50O10S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C36H46O10S2;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 65 ℃;
for 3h;
propargyl bromide;
In
tetrahydrofuran; toluene; mineral oil;
at 65 ℃;
for 16h;
DOI:10.1002/anie.201210090
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / N,N-dimethyl-formamide / 16 h / 50 °C / Inert atmosphere
2.1: sodium hydride / tetrahydrofuran; mineral oil / 3 h / 65 °C
2.2: 16 h / 65 °C
With
tetrakis(triphenylphosphine) palladium(0); sodium hydride; potassium carbonate;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/anie.201210090
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / N,N-dimethyl-formamide / 16 h / 50 °C / Inert atmosphere
2.1: sodium hydride / tetrahydrofuran; mineral oil / 3 h / 65 °C
2.2: 16 h / 65 °C
With
tetrakis(triphenylphosphine) palladium(0); sodium hydride; potassium carbonate;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/anie.201210090