C₂₃H₃₄OS

Base Information

• Chemical Name: C₂₃H₃₄OS
• CAS No.: 1246922-06-4
• Molecular Formula: C₂₃H₃₄OS
• Molecular Weight: 358.588
• Mol file: 1246922-06-4.mol

Synonyms:C₂₃H₃₄OS

Chemical Property of C₂₃H₃₄OS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₃H₃₄OS

There total 1 articles about C₂₃H₃₄OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxyphenylboronic acid (5720-07-0) + 2-bromo-3-dodecylthiophene (139100-06-4) → C23H34OS (1246922-06-4)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; In 1,2-dimethoxyethane; water; for 15h; Reflux;

DOI:10.1002/anie.200903247

Reference yield: 30.0%

C23H34OS (1246922-06-4) → 4,4'-didodecyl-5,5'-bis(4-methoxyphenyl)-2,2'-bithiophene

Guidance literature:

C₂₃H₃₄OS; With n-butyllithium; In tetrahydrofuran; hexane; at -60 ℃; for 0.5h; Inert atmosphere;

With copper dichloride; In tetrahydrofuran; hexane; at -60 - 20 ℃; Inert atmosphere;

DOI:10.1002/anie.200903247

Reference yield:

C23H34OS (1246922-06-4) → C23H33BrOS (1246922-04-2)

Guidance literature:

With N-Bromosuccinimide; In tetrahydrofuran; at 0 - 5 ℃; for 15h;

DOI:10.1002/anie.200903247

upstream raw materials:

4-methoxyphenylboronic acid

2-bromo-3-dodecylthiophene

Downstream raw materials:

C₂₃H₃₃BrOS

Refernces