phenyl 2-phenylpropyl sulfone

Base Information

• Chemical Name: phenyl 2-phenylpropyl sulfone
• CAS No.: 70738-48-6
• Molecular Formula: C₁₅H₁₆O₂S
• Molecular Weight: 260.357
• Mol file: 70738-48-6.mol

Synonyms:phenyl 2-phenylpropyl sulfone

Chemical Property of phenyl 2-phenylpropyl sulfone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of phenyl 2-phenylpropyl sulfone

There total 11 articles about phenyl 2-phenylpropyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(1-Benzenesulfonyl-2-phenyl-propyl)-trimethyl-silane (343621-05-6) → phenyl 2-phenylpropyl sulfone (70738-48-6)

Guidance literature:

With potassium fluoride; In methanol; at 60 ℃; for 0.166667h;

DOI:10.1246/cl.1980.331

Reference yield: 83.0%

(E)-((2-phenylprop-1-en-1-yl)sulfonyl)benzene (64329-88-0) → phenyl 2-phenylpropyl sulfone (70738-48-6)

Guidance literature:

With copper (II)-fluoride; tributylphosphine; phenylsilane; In sodium hydroxide; benzene; at 20 ℃; for 12h;

DOI:10.1002/anie.200701367

Reference yield:

(Z)-((2-phenylprop-1-en-1-yl)sulfonyl)benzene (64329-89-1) → phenyl 2-phenylpropyl sulfone (70738-48-6)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; under 1500.15 Torr; Inert atmosphere;

DOI:10.1021/ja5079877

upstream raw materials:

thiophenol

isopropenylbenzene

(1-Benzenesulfonyl-2-phenyl-propyl)-trimethyl-silane

(Z)-1-phenylthio-1-trimethylsilyl-2-phenylethylene

Refernces

• 1、 Desrosiers, Jean-Nicolas,Charette, Andre B.. "Catalytic enantioselective reduction of β,β-disubstituted vinyl phenyl sulfones by using bisphosphine monoxide ligands". . p. 5955 - 5957. Retrieved 2008/09/17.