Technology Process of C31H49N5O3Si2
There total 16 articles about C31H49N5O3Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
at 0 - 5 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium triethylborohydride / tetrahydrofuran / -78 °C
2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
With
lithium triethylborohydride; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
2: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2011.11.073
- Guidance literature:
-
Multi-step reaction with 4 steps
1: palladium 10% on activated carbon; water; hydrogen; boric acid / tetrahydrofuran / 760.05 Torr
2: methanesulfonyl chloride; triethylamine / dichloromethane
3: lithium triethylborohydride / tetrahydrofuran / -78 °C
4: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
With
palladium 10% on activated carbon; water; hydrogen; boric acid; lithium triethylborohydride; methanesulfonyl chloride; triethylamine; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane;
4: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2011.11.073